A kind of preparation method and use of activated carbon-based inorganic-organic composite material
A composite material, activated carbon technology, applied in chemical instruments and methods, other chemical processes, adsorbed water/sewage treatment, etc., to achieve the effects of low energy consumption, abundant resources, and no ion leakage
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Embodiment 1
[0033] Weigh 10 g of petroleum coke activated carbon and add it to 100 mL of 20% nitric acid solution, stir in a constant temperature water bath at a temperature of 50°C for 24 hours, wash until the pH value is 4-5, and dry at a temperature of 100°C to obtain acidified petroleum coke activated carbon;
[0034]Weigh 100g of sepiolite and add it to 500mL of 20% sulfuric acid solution, stir in a constant temperature water bath at 80°C for 24 hours, wash until the pH value is 4-5, and dry at 100°C to obtain acidified sepiolite;
[0035] Weigh 10 g of acidified petroleum coke activated carbon and add it to 100 mL of a mixed solvent with a volume concentration of 5% ethanol and 95% water, and stir for 5 hours to obtain an activated carbon dispersion solution;
[0036] Weigh 50 mL of activated carbon dispersion solution, add 1 g of hydroxyapatite, 1 g of iron oxyhydroxide, 1 g of titanium dioxide and 1 g of acidified sepiolite, adjust the pH of the mixed solution to 6-7 with hydrochlo...
Embodiment 2
[0041] Weigh 10g of bamboo-based activated carbon and add it to 100mL of 20% sulfuric acid solution, stir in a constant temperature water bath at a temperature of 50°C for 24 hours, wash until the pH value is 4-5, and dry at a temperature of 100°C to obtain acidified bamboo-based activated carbon;
[0042] Weigh 100 g of bentonite and add it to 500 mL of 20% nitric acid solution, stir in a constant temperature water bath at 80°C for 24 hours, wash until the pH value is 4-5, and dry at 100°C to obtain acidified bentonite;
[0043] Weigh 10 g of acidified bamboo-based activated carbon and add it to 100 mL of a mixed solvent with a volume concentration of 5% ethanol and 95% water, and stir for 5 hours to obtain a dispersed solution of activated carbon;
[0044] Weigh 50 mL of activated carbon dispersion solution, add 1 g of hydroxyapatite, 1 g of iron oxyhydroxide, 1 g of titanium dioxide and 1 g of acidified bentonite, adjust the pH of the mixed solution to 6-7 with hydrochloric ...
Embodiment 3
[0049] Weigh 10g of fruit shell activated carbon and add it to 100mL of 20% hydrochloric acid solution, stir in a constant temperature water bath at a temperature of 50°C for 24 hours, wash until the pH value is 4-5, and dry at a temperature of 100°C to obtain acidified shell activated carbon;
[0050] Weigh 100 g of kaolin and add it to 500 mL of 20% phosphoric acid solution, stir in a constant temperature water bath at 80°C for 24 hours, wash until the pH value is 4-5, and dry at 100°C to obtain acidified kaolin;
[0051] Weigh 10 g of acidified fruit shell activated carbon and add it to 100 mL of a mixed solvent with a volume concentration of 5% ethanol and 95% water, and stir for 5 hours to obtain an activated carbon dispersion solution;
[0052] Weigh 50 mL of activated carbon dispersion solution, add 1 g of hydroxyapatite, 1 g of iron oxyhydroxide, 1 g of titanium dioxide and 1 g of acidified kaolin, adjust the pH of the mixed solution to 6-7 with hydrochloric acid, and s...
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