A kind of magnesium-loaded biochar and its preparation method and application
A biochar, magnesium chloride technology, applied in chemical instruments and methods, water pollutants, other chemical processes, etc., to achieve the effects of low cost, simple operation, and strong arsenic adsorption capacity
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Embodiment 1
[0025] Embodiment 1 A kind of magnesium-loaded biochar
[0026] This example provides a magnesium-loaded biochar, which is prepared by the following method: dry and pulverize rice straw that has passed through a 2mm sieve and MgCl with a concentration of 0.5mol / L 2 The solutions are mixed, and the ratio of impregnation solution to biomass is 200mL:20g. After soaking for 0.5h, sonicate for 2h, and dry at 80°C.
[0027] Put it into a stainless steel tank with a diameter of 5 cm and a height of 8 cm, compact it and cover it, place it in a box-type electric furnace, raise the temperature to 500 °C at a heating rate of 20 °C / min, keep it for 4 hours, cool to room temperature and take it out.
[0028] The prepared material was filtered and washed 10 times with deionized water, dried at 80°C, and then ground through a 100-mesh sieve to obtain the magnesium-loaded biochar composite material BC-Mg0.5.
Embodiment 2
[0029] Embodiment 2 A kind of magnesium-loaded biochar
[0030] This example provides a magnesium-loaded biochar, which is prepared by the following method: dry and pulverize rice straw that has passed through a 2mm sieve and MgCl with a concentration of 2.0mol / L 2 The solutions are mixed, and the ratio of impregnation solution to biomass is 200mL:20g. After soaking for 0.5h, sonicate for 2h, and dry at 80°C.
[0031] Put it into a stainless steel tank with a diameter of 5 cm and a height of 8 cm, compact it and cover it, place it in a box-type electric furnace, raise the temperature to 500 °C at a heating rate of 20 °C / min, keep it for 4 hours, cool to room temperature and take it out.
[0032] The prepared material was filtered and washed 15 times with deionized water, dried at 80°C, and then ground through a 100-mesh sieve to obtain the magnesium-loaded biochar composite material BC-Mg2.0.
[0033] Effect verification
[0034] 1. Physical and chemical properties of adsor...
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