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High-throughput preparation method and applications of material, and apparatus for high-throughput preparation of material

A high-throughput, conveying device technology, applied in the field of materials, can solve the problems of difficulty in control, cannot guarantee only a single variable of cooling rate, a single cooling rate, etc., to achieve the effect of fast cooling rate

Inactive Publication Date: 2017-09-12
CENT SOUTH UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

Although this method can realize the detection of the influence of different cooling rates on the structure and properties of materials, this scheme is restricted by many factors in the actual detection process, and it cannot guarantee that there is only a single variable of cooling rate, so the detection results cannot be guaranteed. the accuracy of
At the same time, the method requires a lot of materials, and the preparation and detection time is long, which causes the cost of the method to be high.
[0004] At present, the cooling methods in the heat treatment process of materials include: water quenching, oil quenching, and cooling in the air. The above cooling methods are all directly cooling the sample in the cooling medium, and the cooling rate is single or difficult to control.

Method used

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[0038] The embodiment of the present invention discloses a high-throughput preparation method of materials, including:

[0039] The material sample is heated and held, and then the held material sample is held in place and cooled from one end of the held material sample.

[0040] This application provides a high-throughput preparation method for materials, which is to heat the material sample and then keep it warm, then keep the material sample in place and cool it from one end, so as to efficiently obtain materials with different microstructures at one time. A collection of materials with high performance and performance is a high-throughput material preparation method.

[0041] In the high-throughput preparation process of materials, the materials are solid state materials in the general sense of the art, including metal materials, ceramic materials and composite materials, and the metal materials are metal materials well known to those skilled in the art, as Preferably, th...

Embodiment 1

[0069] figure 1It is a schematic diagram of the device of the present invention, the output end of the induction coil power supply is connected with the input end of the induction heating transformer, the output end of the induction heating transformer is connected with the induction heating coil, the coil part of the induction heating coil is arranged inside the furnace body, and the nickel-based superalloy The coil part of the induction heating coil is fixed and hung inside the furnace body by a high-temperature rope. The thermocouple is welded to the end face of the sample that needs to test the temperature. The output end of the thermocouple is set outside the furnace body and is displayed with the thermocouple digital display. The input end of the thermocouple digital display is connected to the input end of the temperature control and recording computer. There is an opening in the furnace body, and a pipe is arranged at the opening. The outlet of the pipe is connected to ...

Embodiment 2

[0071] figure 2 It is a schematic diagram of the device of the present invention, the output end of the induction coil power supply is connected with the input end of the induction heating transformer, the output end of the induction heating transformer is connected with the induction heating coil, the nickel-based superalloy is fixed by the coil part of the induction heating coil, and passed through the high temperature Hanging by rope, the thermocouple is welded to the end surface of the sample that needs to test the temperature, the output end of the thermocouple is connected to the input end of the thermocouple digital display, and the output end of the thermocouple digital display is connected to the input end of the temperature control and recording computer. A circulating water tank is arranged directly below the material sample, the outlet of the circulating water tank is connected to the inlet of the circulating water pump, and the outlet of the circulating water pump...

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Abstract

The present invention provides a high-throughput preparation method of a material, wherein a material sample is heated, the heated material sample is subjected to thermal insulation, and the obtained material sample is maintained at the in situ state while cooling is performed on the obtained material sample from one end. According to the present invention, the material collections having different microstructures and properties are prepared in the high-throughput manner by cooling the material sample from one end, wherein the heat dissipating way of the cooling end is the direct heat exchange between the metal material and the cooling medium, such that the cooling rate is rapid; and the longitudinal surface of the material and the other end surface are subjected to relatively less heat dissipating, the sample is subjected to heat dissipating along the longitudinal direction mainly in the heat conduction manner so as to provide the slow cooling rate, and the cooling rate from the bottom portion to the top portion of the sample is gradually reduced, such that a series of different continuous cooling rates are achieved on the one sample so as to obtain the material collections having different microstructures and properties. The present invention further provides an apparatus for high-throughput preparation of a material, and applications of the material in high-throughput structure characterization and mechanical characterization.

Description

technical field [0001] The invention relates to the technical field of materials, in particular to a high-throughput preparation method of materials, its application and a device for high-throughput preparation of materials. Background technique [0002] The cooling rate of materials such as metal materials and ceramic materials during heat treatment will directly affect the microstructure of the material, and ultimately affect the mechanical properties of the material. Therefore, it is very important to study the cooling rate during the heat treatment of metal materials to optimize the heat treatment process and improve the mechanical properties of materials. [0003] At present, the main method for measuring the influence of different cooling rates on the structure and properties of materials is: to prepare samples for the same multiple samples at different cooling rates and to test the structures and properties of these samples respectively. Although this method can real...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N1/42G01N1/44
CPCG01N1/42G01N1/44
Inventor 不公告发明人
Owner CENT SOUTH UNIV
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