Compound cesium fluoborate, nonlinear optical crystal with cesium fluoborate, methods for preparing compound cesium fluoborate and nonlinear optical crystal and application of compound cesium fluoborate and nonlinear optical crystal
A technology of nonlinear optics and cesium fluoroborate, which is applied in the field of compounds, can solve the problems of long-term layered growth habit and limited application of crystal growth period
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Embodiment 1
[0055] Preparation compound:
[0056] According to the reaction formula: CsF+2B 2 o 3 →CsB 4 o 6 F, Compound CsB was synthesized by solid-phase synthesis 4 o 6 F:
[0057] CsF,B 2 o 3 Mix evenly at a molar ratio of 1:3, CsF, H 3 BO 3 Mix evenly at a molar ratio of 2:5, put it into a clean and pollution-free platinum crucible with a volume of 28mL, raise the temperature to 350°C, and keep the temperature for 96 hours to obtain the compound CsB 4 o 6 F.
Embodiment 2
[0059] Preparation compound:
[0060] According to the reaction formula: CsF+4H 3 BO 3 →CsB 4 o 6 F+6H 2 O↑, compound CsB was synthesized by solid phase reaction 4 o 6 F:
[0061] CsF,H 3 BO 3 Mix evenly according to the molar ratio of 2:5, put it into a clean and pollution-free platinum crucible with a volume of 28mL, heat up to 600°C, and keep the temperature for 3 hours to obtain the compound CsB 4 o 6 F.
Embodiment 3
[0063] Preparation compound:
[0064] According to the reaction formula: 12CsHCO 3 +4CsBF 4 →CsB 4 o 6 F+15CsF+6H 2 O↑+12CO 2 ↑, compound CsB was synthesized by solid phase reaction 4 o 6 F:
[0065] CsHCO 3 , CsBF 4 Mix evenly at a molar ratio of 2:3, put it into a platinum crucible, place it in a muffle furnace and raise the temperature to 450°C, and keep the temperature constant for 56 hours to obtain the compound CsB 4 o 6 F.
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