Multilayer film heterostructure and its preparation method and application
A heterostructure, multi-layer film technology, applied to devices applying electro-magnetic effects, thermoelectric devices and instruments only using Peltier or Seebeck effects, etc. , unfavorable spin current detection and other problems, to achieve the effect of increasing the number and expanding the range of materials
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Embodiment 1
[0052] This example is used to illustrate the preparation method of the multilayer film heterostructure provided by the present invention.
[0053] The sample was grown on a GGG substrate (3mm×5mm×0.5mm) with 13 μm YIG(Y 3 Fe 5 o 12 ) film, in which YIG is a ferrimagnetic insulator, and then Cu (3nm), CoPt (5nm), IrMn (8nm), SiO 2 (5nm), among which Cu, CoPt, IrMn adopt DC sputtering method, SiO 2 The radio frequency sputtering method adopted, the vacuum degree of the magnetron sputtering equipment is less than 4.0×10 -5 Pa, the working pressure of argon is 0.5Pa.
[0054] The prepared sample GGG / YIG / Cu(3nm) / CoPt(5nm) / IrMn(8nm) / SiO 2 (5nm) is a multilayer heterogeneous structure, such as figure 2 shown.
Embodiment 2-11
[0056] This embodiment is used to illustrate the measurement effect of the longitudinal spin Seebeck effect measurement device provided by the present invention.
[0057] Adopt the preparation method described in embodiment 1 to prepare described sample, all embodiments all adopt GGG substrate (3mm * 5mm * 0.5mm), wherein the material and thickness of each layer are as follows:
[0058]
[0059] The hysteresis loop of embodiment 2 sample GGG / YIG is as Figure 4 shown. The hysteresis loop shows that YIG is an in-plane film and isotropic in the plane. The hysteresis loop of the sample GGG / YIG is measured by a vibrating sample magnetometer, and the in-plane saturation field is about 30Oe.
Embodiment 3
[0060] Example 3 Sample GGG / Cu(3nm) / CoPt(5nm) / IrMn(8nm) / SiO 2 (5nm) hysteresis loop such as Figure 5 shown. Since Cu has a long spin diffusion length and weak spin-orbit coupling, it is an ideal isolation layer to eliminate the ferromagnetic exchange coupling between the ferromagnetic layers YIG and CoPt. Measurement of sample GGG / Cu(3nm) / CoPt(5nm) / IrMn(8nm) / SiO with a vibrating sample magnetometer 2 The hysteresis loop (5nm) shows that the bias field obviously deviates from the zero field, and the left and right coercive forces are far outside the saturation field of the GGG / YIG sample.
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