Self-adhesion silicon rubber material and preparation method thereof
A silicone rubber and self-adhesive technology, applied in the field of self-adhesive silicone rubber material and its preparation, can solve the problems of cumbersome processing procedures and high requirements on adhesives, and achieve simple and reproducible, good tensile strength and fracture Elongation, good reproducibility
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Embodiment 1
[0040] Step 1: Take 100 parts of dimethyl silicone rubber and add it to a double-roller mill, masticate it at room temperature for 10 minutes, then add 30 parts of precipitated silica and 3 parts of polymeric hydroxyl silicone oil, and knead for 10 minutes to obtain Initially mix the rubber material and store it statically for 12 hours, then re-mix the initial rubber material at room temperature for 10 minutes, add 4 parts of triallyl cyanurate, and continue mixing for 10 minutes to obtain the mixed material, which is stored again for 48 hours. hour, and then the sizing material was re-milled for 10 minutes at room temperature, and the compounded material was molded into a sheet or a block on a tablet press at room temperature; the rotating drum speed of the two-roll mill was set to 200r.min -1 ;
[0041] Step 2. After the formed sheet or block is wrapped in plastic or aluminum foil, place it in the air at room temperature 60 Radiation cross-linking is carried out in the Coγ ...
Embodiment 2
[0043]Step 1. Take 100 parts of methyl vinyl silicone rubber and add it to a double-roller open mill, masticate at room temperature for 5 minutes, then add 50 parts of fumed silica and 7 parts of low-molecular-weight hydroxy silicone oil, and knead for 10 minutes. Obtain the initial rubber mixture, store it statically for 24 hours, then re-mill the initial rubber mixture for 15 minutes at room temperature, add 5 parts of triallyl cyanurate sensitizer, and continue mixing for 10 minutes to obtain the mixed material. Static storage again for 24 hours, and then the sizing material was re-milled for 10 minutes at room temperature, and the compound was molded into a sheet or block on a tablet press at room temperature; the rotating drum speed of the two-roll mill was set at 600r.min -1 ;
[0044] Step 2. After the formed sheet or block is wrapped in plastic or aluminum foil, place it in the air at room temperature 60 Radiation cross-linking is carried out in the Coγ radiation fie...
Embodiment 3
[0046] Step 1. Take 100 parts of methyl vinyl silicone rubber and add it to a double-roller open mill, masticate it at room temperature for 5 minutes, then add 10 parts of fumed silica and 1 part of low-molecular-weight hydroxy silicone oil, and knead for 5 minutes. The initial mixed rubber was obtained and stored for 12 hours, and then the initial mixed rubber was kneaded at room temperature for 15 minutes, 1 part of 1,6-hexanediol diacrylate was added, and the mixing was continued for 7 minutes to obtain the mixed material. Static storage again for 36 hours, and then the sizing material was re-milled for 10 minutes at room temperature again, and the compounded material was molded into a sheet or block on a tablet press at room temperature; the rotating drum speed of the two-roll mill was set at 200r.min -1 ;
[0047] Step 2. After the formed sheet or block is wrapped in plastic or aluminum foil, place it in the air at room temperature 60 Radiation cross-linking is carried ...
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