Application of water-retaining shrinkage-reducing polycarboxylate water-reducer in preparation of high-performance concrete
A high-performance concrete and water-retaining technology, applied in the field of water-reducing agent in the preparation of high-performance concrete and water-retaining shrinkage-reducing polycarboxylate water-reducing agent, can solve the problems of low water-to-binder ratio, large increase in engineering cost, cracking, etc.
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Embodiment 1
[0110] An embodiment of the preparation method of the water-retaining shrinkage-reducing polycarboxylate superplasticizer of the present invention comprises the following steps:
[0111] (1) In a closed autoclave, replace the air in the reactor with high-purity nitrogen repeatedly twice, inject 1mol of propylene alcohol and 0.2g of catalyst NaOH, raise the temperature of the reactor to 100-115°C, and start to slowly add 1mol of ring Oxygen, so that the reaction temperature is controlled within the range of 70°C, the pressure in the kettle is controlled at 0.2MPa, and the amount of ethylene oxide required for dropwise addition is controlled by the decrement method. After the dropwise addition of ethylene oxide is completed, the temperature Controlling at 80°C, the reaction was continued for 5h to obtain an intermediate product with the desired molecular weight.
[0112] (2) Keep the temperature at 80°C, start to slowly add 1mol of glycidol dropwise, and control the dropwise add...
Embodiment 2
[0115] An embodiment of the preparation method of the water-retaining shrinkage-reducing polycarboxylate superplasticizer of the present invention comprises the following steps:
[0116] (1) In a closed autoclave, replace the air in the reactor with high-purity nitrogen repeatedly for 3 times, inject 1mol of prenyl alcohol and 0.5gmol of catalyst KOH, raise the temperature of the reactor to 110°C, and start to slowly add 40mol of ring Oxygen, so that the reaction temperature is controlled within the range of 115°C, the pressure in the kettle is controlled at 0.4MPa, and the amount of ethylene oxide required for dropwise addition is controlled by the decrement method. After the dropwise addition of ethylene oxide is completed, the temperature Controlling at 110°C, the reaction was continued for 2h to obtain an intermediate product with the desired molecular weight.
[0117] (2) Lower the temperature to 80° C., start to slowly add 2 mol of glycidol dropwise, and control the drop...
Embodiment 3
[0120] An embodiment of the preparation method of the water-retaining shrinkage-reducing polycarboxylate superplasticizer of the present invention comprises the following steps:
[0121] (1) In a closed autoclave, replace the air in the reactor with high-purity nitrogen repeatedly twice, inject 1mol of isobutenol and 2g of catalyst potassium carbonate, raise the temperature of the reactor to 115°C, and slowly add 80mol of ethylene oxide dropwise Alkanes, so that the reaction temperature is controlled within the range of 130 °C, the pressure in the kettle is controlled at 0.6MPa, and the amount of ethylene oxide required for dropwise addition is controlled by the decrement method. After the dropwise addition of ethylene oxide is completed, the temperature is controlled at At 120°C, the reaction was continued for 0.5h to obtain an intermediate product with the desired molecular weight.
[0122] (2) Lower the temperature to 80° C., start to slowly add 3 mol of glycidol dropwise, ...
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