Lasioderma serricorne (fabricius) sex pheromone and lure thereof
A technology of tobacco beta and pheromone, applied in the field of tobacco compounds
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[0042] The following is attached picture Examples further describe the present invention in detail.
[0043] 1. Extract food odor compounds
[0044] Take large pieces of tobacco leaves, dry them in the sun, and grind them into powder with a pulverizer. Take 1g of tobacco leaf powder, add 10ml of redistilled n-hexane, and soak for 48 hours. Take the upper layer extract, filter, gas phase-mass spectrometer analysis.
[0045] 2. Identification
[0046] Gas phase analysis conditions: All artificially synthesized sex pheromone compounds are analyzed on Agilent 6890GC-5975MS, the chromatographic column is DB-35 (0.25mm x 30m x 25μm), program program: initial temperature 60°C, keep for 1 minute; the first stage The heating rate is 10°C / min, the final temperature is 180°C, and it is kept for 1 minute; the heating rate of the second stage is 10°C / min, and the final temperature is 250°C, and it is kept for 10 minutes.
[0047] Gas chromatography and mass spectrometry analysis condi...
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