Semidull POY polyester fiber and processing method thereof
A technology of polyester fiber and processing method, applied in the field of semi-dull POY polyester fiber and its processing, to achieve good matting effect, excellent matting effect, and good dispersion
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Embodiment 1
[0038] A kind of processing method of semi-dull POY polyester fiber, its concrete steps are:
[0039] The preparation of the first step modified titanium dioxide:
[0040] Using nano-titanium dioxide powder as raw material, under normal temperature, high-speed stirring and ultrasonic dispersion are carried out in cyclohexane solution, the dispersion time is 2-3 hours, the high-speed stirring speed is 2000-3000 rpm, and then in nitrogen atmosphere, Add toluene diisocyanate, react at a reaction temperature of 85-95°C for 45-60 minutes, after the reaction is completed, then distill under reduced pressure for 45 minutes at 110°C, and then dry the product under reduced pressure at 120°C for 48 hours , to prepare modified titanium dioxide.
[0041] The average particle size of the nano-titanium dioxide powder is 45-65 nanometers, the mass concentration of the nano-titanium dioxide powder in cyclohexane is 35g / L, and the molar ratio of toluene diisocyanate toluene diisocyanate to ti...
Embodiment 2
[0058] A kind of processing method of semi-dull POY polyester fiber, its concrete steps are:
[0059] The preparation of the first step modified titanium dioxide:
[0060] Using nano-titanium dioxide powder as raw material, under normal temperature, high-speed stirring and ultrasonic dispersion are carried out in cyclohexane solution. The dispersion time is 2-3 hours, and the high-speed stirring speed is 2000-3000 rpm, and then in nitrogen atmosphere, Add toluene diisocyanate, react at a reaction temperature of 85-95°C for 45-60 minutes, after the reaction is completed, then distill under reduced pressure at 110°C for 45 minutes, and then dry the product under reduced pressure at 120°C for 48 hours , to prepare modified titanium dioxide.
[0061] The average particle size of the nano-titanium dioxide powder is 45-65 nanometers, the mass concentration of the nano-titanium dioxide powder in cyclohexane is 40 g / L, and the molar ratio of toluene diisocyanate toluene diisocyanate ...
Embodiment 3
[0078] A kind of processing method of semi-dull POY polyester fiber, its concrete steps are:
[0079] The preparation of the first step modified titanium dioxide:
[0080] Using nano-titanium dioxide powder as raw material, under normal temperature, high-speed stirring and ultrasonic dispersion are carried out in cyclohexane solution, the dispersion time is 2-3 hours, the high-speed stirring speed is 2000-3000 rpm, and then in nitrogen atmosphere, Add toluene diisocyanate, react at a reaction temperature of 85-95°C for 45-60 minutes, after the reaction is completed, then distill under reduced pressure for 45 minutes at 110°C, and then dry the product under reduced pressure at 120°C for 48 hours , to prepare modified titanium dioxide.
[0081] The average particle size of the nano-titanium dioxide powder is 45-65 nanometers, the mass concentration of the nano-titanium dioxide powder in cyclohexane is 50 g / L, and the molar ratio of toluene diisocyanate toluene diisocyanate to t...
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