Method for determination of thorium content of thorium dioxide
A technology of thorium dioxide and a determination method, which is applied in the direction of material analysis by observing the influence on chemical indicators, preparation of test samples, and analysis by chemical reaction of materials, etc., can solve the problem of high cost and complicated operation process. and other problems to achieve high precision
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[0025] The present invention will be further described below in conjunction with the accompanying drawings and embodiments.
[0026] Such as figure 1 Shown, a kind of assay method of thorium content in thorium dioxide, specifically comprises the following steps:
[0027] The first step is to decompose the sample.
[0028] Step 1.1: Put the sample in a 50mL beaker, add 10mL of ρ(HNO3)=1.42g / mL high-grade pure nitric acid solution, 0.1mL of ρ(HF)=1.15g / mL high-grade pure hydrofluoric acid The solution is heated to 250°C on a temperature-adjusting electric heating plate until the sample is completely dissolved, then removed and cooled to room temperature. Use deionized water to transfer the sample to a 100mL volumetric flask, dilute to the mark with water, and mix well.
[0029] Step 1.2: Pipette 5.00 mL of the test solution obtained in Step 1.1 into a 300 mL Erlenmeyer flask, add 30 mL of water, adjust the pH of the solution to 1.6-2.0 with 2 mol / L ammonia water, and test wit...
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