Molecular sieve/porous carbon composite electrode material for capacitive adsorption desalination and preparation method thereof
A porous carbon material, capacitive adsorption technology, applied in separation methods, chemical instruments and methods, water/sewage treatment, etc., can solve the problems of reducing desalination efficiency and electrode efficiency, increasing energy consumption, and limiting the application of porous carbon electrode materials, etc. Achieve the effect of facilitating ion diffusion and adsorption, reducing repulsion, and low cost
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Embodiment 1
[0033] Take H-type β molecular sieve HSZ-1 with high silicon content as the doping component, and its properties are as follows: SiO 2 / Al 2 o 3 The molar ratio is 40:1, and the specific surface area is 530m 2 / g, the particle diameter is about 4 microns.
[0034] Preparation concentration is the dispersion liquid (dispersion in deionized water) of 50mg / mL activated carbon and HSZ-1 molecular sieve, adds PTFE emulsion (mass fraction 60%), activated carbon, HSZ-1 molecular sieve and PTFE mass ratio are 90:10:7, After mechanical stirring for 2 hours, dry in an oven at 95°C to obtain a flocculent molecular sieve / activated carbon mixture. A small amount of ethanol was added to the resulting mixture for wetting, rolled into a sheet and pressed on a titanium mesh to obtain an HSZ-1 / activated carbon (HSZ-1 / AC) electrode.
[0035] figure 1 It is the SEM topography image of HSZ-1 / AC electrode.
[0036] Assemble an asymmetric capacitive desalination device, use the molecular siev...
Embodiment 2
[0038] Take Na-type mordenite molecular sieve HSZ-2 with high silicon content as the doping component, and its properties are as follows: SiO 2 / Al 2 o 3 The molar ratio is 18:1, Na 2 O / Al 2 o 3 The molar ratio is 1:1, and the particle diameter is about 12 microns.
[0039] Preparation concentration is the dispersion liquid (dispersion in deionized water) of 50mg / mL activated carbon and HSZ-2 molecular sieve, adds PTFE emulsion (mass fraction 60%), activated carbon, HSZ-2 molecular sieve and PTFE mass ratio are 90:10:7, After mechanical stirring for 2 hours, dry in an oven at 95°C to obtain a flocculent molecular sieve / activated carbon mixture. A small amount of ethanol was added to the obtained HSZ-2 / activated carbon mixture for wetting, rolled into a sheet and pressed on a titanium mesh to obtain an HSZ-2 / activated carbon (HSZ-2 / AC) electrode. image 3 It is the SEM topography of HSZ-2 / AC electrode.
[0040] Assemble an asymmetric capacitive desalination device, use t...
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