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Method for synchronously extracting soybean oil, soybean milk powder and soybean dietary fiber by aqueous enzymatic method

A soybean dietary fiber and simultaneous extraction technology, applied in milk substitutes, dairy products, food science, etc., can solve the problems of high cost of enzyme preparations, difficult demulsification, long reaction time, etc.

Inactive Publication Date: 2016-04-20
NORTHEAST AGRICULTURAL UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the extraction of soybean oil by aqueous enzymatic method is mostly limited to laboratory research. Due to the problems of high cost of enzyme preparation, long reaction time, and difficulty in demulsification in the process of extracting soybean oil by aqueous enzymatic method, it is rarely put into production practice. There are few studies on the simultaneous industrial production of soybean oil, soybean milk powder and soybean dietary fiber by aqueous enzymatic method

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] Dehulling the soybeans and crushing them, then adjusting the moisture content, extruding and puffing under the conditions of material moisture content of 18%, sleeve temperature of 95°C, screw speed of 110r / min, and die hole diameter of 20mm to obtain puffed products; Add water into the hydrolysis reaction kettle, heat it with steam at 55°C, add the puffed product into the heated water and mix to obtain a mixed solution, use 2mol / L NaOH solution to adjust the pH of the mixed solution to 8.5, and carry out alkali extraction on the mixed solution 40min, after alkaline extraction, under the condition that the ratio of solid to liquid is 1:7, add 1.5‰ Alcalase alkaline protease to the mixed solution for enzymolysis for 30min, after enzymolysis, use a three-phase horizontal centrifuge to centrifuge to obtain emulsified oil, Hydrolyzed solution and residue; use a disc centrifuge to centrifuge the emulsified oil to obtain soybean oil and water phase, add the water phase to the ...

Embodiment 2

[0021] Dehulling the soybeans and crushing them, then adjusting the moisture content, extruding and puffing under the conditions of material moisture content of 18%, sleeve temperature of 95°C, screw speed of 110r / min, and die hole diameter of 20mm to obtain puffed products; Add water into the hydrolysis reaction kettle, heat it with steam at 50°C, add the puffed product to the heated water and mix to obtain a mixed solution, use 2mol / L NaOH solution to adjust the pH of the mixed solution to 9, and carry out alkali extraction on the mixed solution 30min, after the alkali extraction, under the condition that the ratio of solid to liquid is 1:8, add 1‰ Alcalase alkaline protease to the mixed solution to carry out enzymolysis for 35min, and after enzymolysis, use a three-phase horizontal centrifuge to carry out centrifugal separation to obtain emulsified oil Hydrolyzed solution and residue; use a disc centrifuge to centrifuge the emulsified oil to obtain soybean oil and water phas...

Embodiment 3

[0023]Dehulling the soybeans and crushing them, then adjusting the moisture content, extruding and puffing under the conditions of material moisture content of 18%, sleeve temperature of 95°C, screw speed of 110r / min, and die hole diameter of 20mm to obtain puffed products; Add water into the hydrolysis reaction kettle, heat it with steam at 60°C, add the puffed product to the heated water and mix to obtain a mixed solution, use 2mol / L NaOH solution to adjust the pH of the mixed solution to 8, and carry out alkali extraction on the mixed solution 50min, after the alkali extraction, under the condition that the ratio of solid to liquid is 1:6, add 2‰ Alcalase alkaline protease to the mixed solution to carry out enzymolysis for 25min. Hydrolyzed solution and residue; use a disc centrifuge to centrifuge the emulsified oil to obtain soybean oil and water phase, add the water phase to the hydrolyzed solution and mix evenly, then vacuum concentrate in the concentration tower, and spr...

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PUM

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Abstract

The invention relates to a method for synchronously extracting soybean oil, soybean milk powder and soybean dietary fiber by an aqueous enzymatic method, which belongs to the technical field of plant grease processing. The method comprises the following steps: 1) dehulling soybeans and crushing the soybeans, extruding and puffing the material to obtain a puffed product; 2) adding water into an enzymatic hydrolysis reaction vessel, heating steam and adding the puffed product to obtain a mixed liquor, performing alkaline extraction on the mixed liquor, adding alkali protease for performing enzymatic hydrolysis, using a horizontal centrifuge after enzymatic hydrolysis is carried out for performing centrifugation to obtain an emulsified oil, a hydrolysate and residues; 3) using a disk centrifuge for performing centrifugation on the emulsified oil to obtain the soybean oil and a water phase, adding the water phase into the hydrolysate for concentration, and drying the material to obtain the soybean milk powder; and 4) adding water for mixing the water and the residues for homogenizing and drying a mixture to obtain the soybean dietary fiber. The method has the advantages of simple process, less enzyme usage amount, short reaction time, and low cost. The prepared high-quality soybean oil can obtain the high-nutrition partly-defatted soybean milk powder and high-oil high-protein soybean dietary fiber, and is suitable for industrial continuous production.

Description

technical field [0001] The invention belongs to the technical field of vegetable oil processing, and mainly relates to a method for synchronously extracting soybean oil, soybean milk powder and soybean dietary fiber by an aqueous enzymatic method. Background technique [0002] The traditional methods of producing vegetable oil are mainly pressing and leaching. The pressing method has a simple process and less supporting equipment, which can maintain the special flavor of the product, but the oil extraction rate is low, the energy consumption is high, and the cost is high. Moreover, the protein denaturation of the cake after pressing is serious, and the protein utilization rate is low, resulting in a serious waste of vegetable protein. . The leaching method has high production efficiency and low residual oil rate, but this method requires a lot of equipment, large investment, large loss of oil flavor and residual organic solvents, and requires refining treatment, and also po...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B1/04C11B1/00A23C11/10A23L33/22A23L11/65
CPCA23C11/103C11B1/00C11B1/025C11B1/04
Inventor 江连洲齐宝坤李杨隋晓楠王中江
Owner NORTHEAST AGRICULTURAL UNIVERSITY
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