Dried tangerine or orange peel tea dropping pill and preparation method thereof
A technology for tea dripping pills and tangerine peel, which is applied in the field of health-care tea preparation, can solve the problems of difficult extraction of effective components of tangerine peel tea, and the difficulty of carrying tangerine peel tea, and achieves the effects of improving utilization value, being convenient for production and carrying, and being convenient to use.
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[0022] The present invention also provides a kind of preparation method of tangerine peel tea dripping pill, comprises the following steps:
[0023] Step 1. Preparation of tangerine peel extract concentrate: remove impurities, wash and dry tangerine peel, sterilize by sunlight, stir fry and crush, add water, adjust pH to 8-10, add to CO 2 In the supercritical extractor, ethanol is used as an entrainer, and the volume percentage of the entrainer in the total extraction solvent is 12-15%, the extraction pressure is 55-65MPa, the temperature is 45-60°C, CO 2 The flow rate is 3-5m1 / g crude drug.min, the extraction time is 4-8h, to obtain supercritical extract, add 95% ethanol solution, soak for 20h-28h, heat and reflux for 2h-3h, and then filter under normal temperature and pressure to obtain leaching The extract is concentrated under reduced pressure to obtain a dark green extract, which is the ethanol extract, concentrated, added to the LSA-900C macroporous adsorption resin colu...
Embodiment 1
[0030] A method for preparing tangerine peel tea dripping pills, comprising the following steps: removing impurities, washing tangerine peel, drying in the sun, sterilizing by sunlight, frying and pulverizing, adding water, adjusting pH to 9, adding CO 2 In the supercritical extractor, ethanol is used as an entrainer, and the volume percentage of the entrainer in the total extraction solvent is 14%, the extraction pressure is 60MPa, the temperature is 55°C, and the CO 2The flow rate is 4m1 / g crude drug.min, the extraction time is 6h, and the supercritical extract is obtained. Add 95% ethanol solution, soak for 24h, heat and reflux for 2.5h, and then filter under normal temperature and pressure to obtain the leaching solution. Concentrate under reduced pressure to obtain a dark green extract, which is the ethanol extract, concentrate, add to an LSA-900C macroporous adsorption resin column, elute with 50% ethanol, collect 6 times the column volume eluate, and recover ethanol unde...
Embodiment 2
[0032] A method for preparing tangerine peel tea dripping pills, comprising the following steps: removing impurities, washing tangerine peel, drying in the sun, sterilizing by sunlight, frying and pulverizing, adding water, adjusting pH to 8, adding CO 2 In the supercritical extractor, ethanol is used as an entrainer, and the volume percentage of the entrainer in the total extraction solvent is 12%, the extraction pressure is 55MPa, the temperature is 45°C, and CO 2 The flow rate is 3m1 / g crude drug.min, the extraction time is 4h, and the supercritical extract is obtained. Add 95% ethanol solution, soak for 20h, heat and reflux for 2h, and then filter under normal temperature and pressure to obtain the leaching solution, and reduce the leaching solution. Concentrate under pressure to obtain a dark green extract, which is the ethanol extract, concentrate, add to LSA-900C macroporous adsorption resin column, elute with 50% ethanol, collect 6 times the column volume eluate, recove...
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