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A method for preparing electronic cigarette liquid by microwave-assisted extraction

An electronic cigarette liquid, microwave-assisted technology, applied in solid solvent extraction, chemical instruments and methods, tobacco and other directions, can solve the problems of non-smoking materials affecting the traditional smoking taste of tobacco, high manufacturing cost, environmental pollution, etc. , The effect of small reagent dosage and high thermal efficiency

Inactive Publication Date: 2017-03-29
立场电子科技发展(上海)有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0010] CN102972862A discloses a tobacco raw material improvement process and its equipment, the purpose of which is to solve the complex process and high manufacturing cost of the existing improved technology, and the safety problems caused by the addition of non-smoke materials will affect the traditional smoking of tobacco and cause environmental pollution. Defects such as pollution; key points of the technical plan: the process sequentially uses mixed solvents to perform specific extraction on more than one of tobacco leaves, tobacco sheets, shredded tobacco, tobacco powder, tobacco stems, and shredded stems, and the extracted tobacco raw materials are subjected to specific solid-liquid separation The extract of tobacco leaves, tobacco sheets or shredded tobacco is used to prepare tobacco extract, and the extract of tobacco stem or shredded stem is used to make fertilizer. A specific amount of tobacco water extract and tobacco alcohol extract is diluted and mixed, After separating the bad components, it is formulated into a backfill liquid, and the backfill liquid is evenly backfilled on the tobacco raw material, and then dried to a specific moisture content to obtain the finished product

Method used

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  • A method for preparing electronic cigarette liquid by microwave-assisted extraction
  • A method for preparing electronic cigarette liquid by microwave-assisted extraction

Examples

Experimental program
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Effect test

Embodiment 1

[0041] Repeat the above specific implementation steps, wherein the extraction solvent is preferably methanol:n-hexane=1:8, the microwave power is preferably 350W, the radiation time is preferably 5min, the tobacco leaf extract is preferably 50%, the tobacco essence is preferably 2%, and the deionized water is preferably 2%. Natural nicotine is preferably 1%. The ratio of the selected tobacco leaf mixture is: in parts by weight, 10 parts of Yunnan Yuxi fragrance tobacco leaves, 15 parts of Yunnan Dali fragrance tobacco leaves, and 15 parts of Yunnan Qujing fragrance tobacco leaves.

Embodiment 2

[0043] Repeat the above specific implementation steps, wherein the extraction solvent is preferably methanol:petroleum ether=1:5, the microwave power is preferably 500W, the radiation time is preferably 6min, the tobacco leaf extract is preferably 50%, the tobacco essence is preferably 1%, and the tobacco flavor is preferably 1%, Deionized water is preferably 2%, and natural nicotine is preferably 1%. The ratio of the selected tobacco leaf mixture is: in parts by weight, 10 parts of Yunnan Yuxi fragrance tobacco leaves, 10 parts of Yunnan Dali fragrance tobacco leaves, and 15 parts of Yunnan Qujing fragrance tobacco leaves.

Embodiment 3

[0045] Repeat the above specific implementation steps, wherein the extraction solvent is preferably methanol:petroleum ether=1:6, the microwave power is preferably 650W, the radiation time is preferably 4min, the tobacco leaf extract is preferably 40%, the tobacco essence is preferably 2%, and the tobacco flavor is preferably 2%, Deionized water is preferably 1%, and natural nicotine is preferably 1%. The ratio of the selected tobacco leaf mixture is: in parts by weight, 15 parts of Yunnan Yuxi fragrance tobacco leaves, 20 parts of Yunnan Dali fragrance tobacco leaves, and 20 parts of Yunnan Qujing fragrance tobacco leaves.

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Abstract

The invention discloses a method for preparing an electronic cigarette liquid through microwave-assisted extraction. An extraction liquid and mixed tobacco leaves are mixed and irradiated by microwaves, organic phases are merged after filtering and washing operation, an organic solvent is finally removed, and a tobacco leaf extract is obtained, wherein the extraction liquid and the mixed tobacco leaves are mixed in the weight ratio being (1:1)-(5:1); the adopted power is 400-800 W during microwave irradiation; the faint-scent tobacco leaf extract is prepared from Yunnan Yuxi faint-scent tobacco leaves, Yunnan Dali faint-scent tobacco leaves and Yunnan Qujing faint-scent tobacco leaves. By comparison with conventional extraction methods such as a room-temperature extraction method and a heating reflux method, the extraction time is greatly shortened, the use quantity of solvents is reduced, and the extraction efficiency is remarkably improved. Besides, the extract is prepared from mixed tobacco leaf extracts, and different tobacco leaf extracts complement each other in scent, so that the scent and the taste of the electronic cigarette liquid are more close to those of conventional cigarettes.

Description

technical field [0001] The invention relates to a method for preparing electronic cigarette liquid by using microwave-assisted extraction. It belongs to the field of tobacco chemical industry. Background technique [0002] E-cigarettes are currently a widely popular alternative to cigarettes. There have been many literature and patent reports on the preparation and preparation of e-liquid in e-cigarettes. [0003] In order to imitate the original flavor of traditional cigarettes, a method of preparing e-cigarette liquid by using tobacco leaf extracts combined with tobacco flavors and flavors has been developed. For example, a preparation method of electronic cigarette liquid (patent application No. 201110184068.6), a flue-cured tobacco type electronic cigarette liquid (patent application No. 201110263484.5), an electronic cigarette liquid that can effectively improve the sensory quality of electronic cigarettes (patent application No. ) and so on disclosed the preparation...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A24B15/26A24F47/00B01D11/02
CPCA24B15/26A24F47/004B01D2259/806
Inventor 林嘉宇
Owner 立场电子科技发展(上海)有限公司
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