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Method for increasing synthetic ratio in hair hydrolyzation for preparing aquatic ecological protecting agent

A technology of synthesis rate and water ecology, applied in water/sewage treatment, chemical instruments and methods, water/sludge/sewage treatment, etc., can solve the problems of slow enzymatic hydrolysis process, high equipment requirements, amino acid damage, etc. The effect of increasing the reaction rate, shortening the reaction time, and increasing the synthesis rate

Active Publication Date: 2016-02-03
临沭县益兴供汽维修服务有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the main methods of hydrolyzing hair are high-temperature and high-pressure hydrolysis, acid-base hydrolysis, and enzymatic hydrolysis. However, since high-temperature and high-pressure hydrolysis is generally at 170-370°C, the hydrolyzed amino acids are easily damaged at high temperatures, and even Carbonization; Acid-base hydrolysis generally uses strong acid and strong alkali, which requires high equipment and corrosion resistance. At the same time, the hydrolysis time is generally 8-12 hours; the enzymatic hydrolysis process is slow and takes a long time

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] A method for improving hair hydrolysis synthesis rate to prepare water ecological protection agent, comprising the following steps:

[0026] 1) Clean the hair, dry it in an oven until the moisture content of the hair is 10%, crush the hair to a length of 10 μm, add keratinase and deionized water under normal temperature at a pressure of 20 Mpa, and keep stirring for 10 minutes. Obtain mixed solution A; wherein the hair, keratinase and deionized water have a ratio of parts by weight of 100:5:100, and the hair used for hydrolysis is first pulverized into small pieces to increase the reaction contact area, which is beneficial to accelerate the rate of hair hydrolysis reaction, The added keratinase can first decompose the keratin in the hair into polypeptides. Under high pressure, the speed of keratinase decomposing keratin can be accelerated. It does not need to be carried out at high temperature. The hair or the decomposed polypeptides will not be carbonized and will not d...

Embodiment 2

[0030] A method for improving hair hydrolysis synthesis rate to prepare water ecological protection agent, comprising the following steps:

[0031]1) Clean the hair, dry it in an oven until the moisture content of the hair is 20%, crush the hair to a length of 20 μm, add keratinase Trichophyton monkeyis and deionized water under the pressure of 30Mpa at room temperature, and keep stirring Reacted for 20 minutes, wherein the speed of stirring was 100rmp, to obtain mixed solution A; wherein the weight and number ratio of the hair, keratinase and deionized water was 150:10:150, and the pH of the deionized water was 8. The hair used for hydrolysis is first crushed into small pieces to increase the reaction contact area, which is beneficial to speed up the rate of hair hydrolysis reaction. The added keratinase can first decompose the keratin in the hair into polypeptides, and can accelerate the decomposition of keratin by keratinase under high pressure. The speed does not need to b...

Embodiment 3

[0035] A method for improving hair hydrolysis synthesis rate to prepare water ecological protection agent, comprising the following steps:

[0036] 1), clean the hair, dry it in an oven until the moisture content of the hair is 15%, crush the hair to a length of 15 μm, add keratinase Trichophyton monkey, Trichophyton sp. Aspergillus and deionized water, constantly stirring reaction 15 minutes, wherein the speed of stirring is 75rmp, obtains mixed solution A; Wherein said hair, keratinase Trichophyton simiensis, Cyclospora bacterium, Aspergillus fumigatus and the weight of deionized water The ratio of parts and numbers is 125:7:125, the pH value of the deionized water is 9, and the hair used for hydrolysis is first crushed into small pieces to increase the reaction contact area, which is beneficial to accelerate the rate of hair hydrolysis reaction, and the added keratinase can detoxify the hair The keratin in the product is first decomposed into polypeptides, and the speed of ...

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PUM

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Abstract

The invention discloses a method for increasing a synthetic ratio in hair hydrolyzation for preparing an aquatic ecological protecting agent. The method comprises the following steps: 1) cleaning, drying and crushing hair, adding keratinase and deionized water and reacting to obtain a solution A under the pressure of 20 to 30 Mpa and normal temperature; 2) selecting one or more of salicylic acid, adipic acid, malonic acid, succinic acid and palmic acid and uniformly mixing with the deionized water to prepare a solution, reacting the obtained solution with the solution A at 10 to 20Mpa and at 30 to 40 DEG C, and filtering to obtain a solution B; 3) selecting one or more of ethylene diamine tetra (methylene phosphonic acid) sodium, diethylenetriaminepenta(methylenephosphonic) acid, amino trimethylene phosphonic acid, tartaric acid, heptonate, sodium gluconate and sodium alginate and uniformly mixing with the deionized water, and then uniformly mixing with the solution B to obtain a finished product. According to the method disclosed by the invention, the time of hair hydrolyzation is shortened, the extraction rate of hair hydrolyzation into amino acids is increased, and therefore the synthetic rate of synthesizing the aquatic ecological protecting agent is increased.

Description

technical field [0001] The invention relates to the technical field of preparation of water ecological protection agents. More specifically, the present invention relates to a method for improving the synthesis rate of hair hydrolysis to prepare water ecological protection agent. Background technique [0002] In the process of aquaculture, the use of chemical drugs to control the disease will not only increase the cost of breeding, but also lead to a decline in product quality and serious environmental pollution. With the progress and development of economy and technology, people's awareness of environmental protection has gradually increased, and the requirements for product quality have also increased, and more and more attention has been paid to environmental pollution. In recent years, hair hydrolyzate has been used as the main component of water ecological protection agents. In industrialized production, it is usually used in the middle and late stages of cultivation a...

Claims

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Application Information

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IPC IPC(8): C02F1/00
Inventor 苏兴建庞鈜苏铭龙李远华庞兴惠张以光曹丽伟
Owner 临沭县益兴供汽维修服务有限公司
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