Novel Cr-Y-O nanocluster oxide dispersion strengthening reduced activation steel
A low-activation steel, dispersion-strengthening technology, applied in the field of anti-irradiation metal materials, can solve the problem that it is easy to be adsorbed on the surface of powder particles, the oxygen content of the oxide dispersion-strengthened low-activation steel matrix cannot be effectively controlled, and the specific surface area of powder particles cannot be effectively controlled. It can achieve low activation performance, good anti-irradiation swelling ability, and the effect of reducing oxygen content
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Embodiment 1
[0032] The mass percent of the alloying elements of the oxide dispersion strengthened steel is: 0.041%C, 13.88%Cr, 1.35%W, 0.19%V, 0.07%Ta, 0.41%Mn, 0.10%Si, 0.74%Y, 73(ppm ) N, 64 (ppm) Al, 48 (ppm) Ni, 48 (ppm) Mo, 65 (ppm) Nb, Cu<0.010%, P<0.005%, S<0.005%, and the matrix is Fe.
[0033] Preparation method: First, prepare Cr-Y ball mill powder (the mass ratio of Cr-Y pure metal powder is Cr:Y=9:1, the ball milling medium is Φ6 hard steel balls, the ball milling atmosphere is 99.99% argon, and the mass ratio of ball to material is is 10:1, the ball milling time is 4h, and the rotating speed is 1425r / min), and then the Cr-Y ball mill powder (the scanning electron microscope photo is shown in figure 2 As shown) is added to Fe-C-Cr-W-V-Ta-Mn-Si steel powder for high-energy ball milling (the ball milling medium is Φ6 and Φ10 mixed hard steel balls, the ball milling atmosphere is 99.99% argon, and the mass ratio of balls to materials is 10 : 1, ball milling time 70h, rotating...
Embodiment 2
[0035] The alloy element content of the oxide dispersion strengthened steel is the same as that of the steel of Example 1.
[0036] Preparation method: First, prepare Cr-Y ball mill powder (the mass ratio of Cr-Y pure metal powder is Cr:Y=9:1, the ball milling medium is Φ6 hard steel balls, the ball milling atmosphere is 99.99% argon, and the mass ratio of ball to material is 10:1, ball milling time 4h, rotating speed 1425r / min), then add Cr-Y ball mill powder into Fe-C-Cr-W-V-Ta-Mn-Si steel powder for high-energy ball milling (ball milling medium is Φ6 and Φ10 Mix hard steel balls, the ball milling atmosphere is 99.99% argon, the mass ratio of balls to material is 10:1, the ball milling time is 70h, and the rotating speed is 450r / min). Secondly, the mixed powder is first packed into a bag and evacuated (vacuum degree 10 -1 Pa, temperature 450°C, time 4h), and then cured by hot isostatic pressing (pressure 130MPa, temperature 1050°C, holding time 3h). Finally, after preparin...
Embodiment 3
[0038] The difference from Example 1 is that the heat treatment system is different: normalizing at 1150-1200°C / 50min / air cooling + tempering at 820°C / 90min / air cooling, finally obtaining oxide dispersion strengthened low activation steel.
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