Plant source herbicide and preparation method thereof
A technology of herbicides and botanical sources, applied in the field of botanical herbicides and their preparation, to achieve the effects of reducing residues, easy degradation, and convenient material extraction
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Embodiment 1
[0039] 1. Wash the collected Hainan staghorn vine, dry it in the shade indoors, crush it, pass through a 40-mesh sieve, then add methanol 5 times the volume of the dry powder and extract it in a dark place for 3 days, and repeatedly extract it 3 times. The extracts were combined, concentrated under reduced pressure at 45°C to form a paste, and the methanol extract of S. hainanensis was obtained, which was stored in a refrigerator at 4°C for later use.
[0040] 2. According to the ratio of methanol extract of Hainan staghorn vine 0.1%, methanol 5%, sodium lauryl sulfate 3%, Nongru No. 300 2%, benzoic acid 0.5%, vitamin E 0.5%, and the balance is water . Take by weighing 10g methanol extract of hainan staghorn vine, 500ml methanol, mix and stir evenly, and set aside; 300g sodium lauryl sulfate, 200g Nongru No. 300 and 2000ml water are mixed and stirred, then added to the methanol containing extract, and then Add 5g of benzoic acid, 5g of vitamin E and the water of surplus, stir...
Embodiment 2
[0042] 1. Wash the collected Hainan staghorn vine, dry it in the shade indoors, crush it, pass through a 50-mesh sieve, add methanol 4 times the volume of the dry powder, and extract it in a dark place for 4 days, and repeatedly extract it twice. The extracts were combined, concentrated under reduced pressure at 40°C to form a paste, and the methanol extract of S. hainanensis was obtained, which was stored in a refrigerator at 4°C for later use.
[0043] 2. According to the ratio of Hainan staghorn vine methanol extract 1%, methanol 7%, Nongru No. 700 6%, sodium lignosulfonate 4%, sorbic acid 0.5%, vitamin E 0.5%, and the balance is water. Weigh 10g methanol extract of hainan staghorn vine, 70ml methanol, mix and stir; 60g Nongru No. 700, 40g sodium lignosulfonate and 300ml water are mixed and stirred, then added to the methanol containing extract, and then 5g sorbic acid , 5g vitamin E and the water of surplus, stir at high speed, obtain the microemulsion product, pass inspec...
Embodiment 3
[0045] 1. Wash the collected Hainan staghorn vine, dry it naturally in the shade, crush it, and pass it through a 60-mesh sieve, then add 6 times the volume of dry powder to leaching in a dark place for 2 days, and repeatedly leaching 4 times. The extracts were combined, concentrated under reduced pressure at 50°C to form a paste, and the methanol extract of S. hainanensis was obtained, which was stored in a refrigerator at 4°C for later use.
[0046] 2. According to Hainan staghorn vine methanol extract 5%, n-butanol 10%, nonylphenol polyoxyethylene ether 8%, lauryl calcium sulfate 2%, citric acid 1%, tertiary butyl hydroquinone 1%, The balance is the proportion of water. Weigh 50g methanol crude extract of staghorn vine, 100ml n-butanol, mix and stir; 80g nonylphenol polyoxyethylene ether, 20g lauryl calcium sulfate and 400ml water are mixed and stirred, and then added to the n-butanol containing extract , add 10g citric acid, 10g tert-butyl hydroquinone and the water of su...
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