Novel water pipe joint nanometer waterproof film production process
A technology of waterproof film and water pipe joints, applied in the direction of coating, etc., to improve suspension stability, reduce costs, and ensure waterproof and anti-seepage effects
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Embodiment 1
[0037] A new type of production process of nano waterproof film for water pipe joints, the process is as follows:
[0038] (1) Preparation of basic membrane
[0039] ① Mix 31 parts by mass of nano-silica, 26 parts by mass of nano-titania and 12 parts by mass of nano-zinc oxide, stir and mix at a speed of 150r / min for 30 minutes to obtain a nano main material;
[0040] ② Put 7 parts by mass of silicone-acrylic emulsion into the stirring tank, gradually add 4 parts by mass of butyl acrylate, control the temperature at 63°C, and stir and mix at 160r / min for 45min to obtain the bottom solvent;
[0041] ③Take the nano main material obtained in step (1)①, and gradually add it to the bottom solvent obtained in step (1)②, control the temperature at 55℃, stir and mix at 220r / min for 1.5h, during which 4 parts by mass are added Sodium carboxymethyl cellulose and 2 parts by mass of organosilicon defoamer to obtain film raw materials;
[0042] ④The film raw material is molded by a molding machine,...
Embodiment 2
[0050] A new type of production process of nano waterproof film for water pipe joints, the process is as follows:
[0051] (1) Preparation of basic membrane
[0052] ① Mix 30 parts by mass of nano-silica, 15 parts by mass of nano-titania and 14 parts by mass of nano-zinc oxide, stirring and mixing at a speed of 130r / min for 40 minutes to obtain a nano main material;
[0053] ② Put 17 parts by mass of silicone-acrylic emulsion into the stirring tank, gradually add 7 parts by mass of butyl acrylate, control the temperature at 75°C, and stir and mix at 140r / min for 35min to obtain the bottom solvent;
[0054] ③Take the nano main material obtained in step (1) ①, and gradually add it to the bottom solvent obtained in step (1) ②, control the temperature at 58 ℃, stir and mix at 180r / min for 1 hour, and add 5 parts by mass of carboxylate during this period. Sodium methylcellulose and 2 parts by mass of organosilicon defoamer to obtain film raw materials;
[0055] ④The film raw material is mol...
Embodiment 3
[0062] A new type of production process of nano waterproof film for water pipe joints, the process is as follows:
[0063] (1) Preparation of basic membrane
[0064] ① Mix 22 parts by mass of nano-silica, 28 parts by mass of nano-titania and 9 parts by mass of nano-zinc oxide, stirring and mixing at a speed of 130r / min for 25min to obtain a nanometer main material;
[0065] ② Put 18 parts by mass of silicone-acrylic emulsion into the stirring tank, gradually add 6 parts by mass of butyl acrylate, control the temperature at 70°C, and stir and mix at 150r / min for 45min to obtain the bottom solvent;
[0066] ③Take the nano main material obtained in step (1)①, and gradually add it to the bottom solvent obtained in step (1)②, control the temperature at 48℃, stir and mix at 250r / min for 1h, during which 6 parts by mass of polymer are added. Vinyl alcohol and 3 parts by mass of organosilicon defoamer to obtain film raw materials;
[0067] ④The film raw material is molded by a molding machine,...
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