Low-loss soft magnetic ferrite material and preparation method thereof
A technology of soft ferrite and low loss, which is applied in the field of low loss soft ferrite material and its preparation, can solve the problem of unsatisfactory magnetic core loss, etc., and achieve high magnetic permeability, high resistivity, and high magnetic permeability Effect
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[0027] refer to figure 1 , the preparation method of a kind of low-loss soft magnetic ferrite material that the present invention proposes, comprises the following steps:
[0028] S1. After adding the adsorbent and emulsifier into the water and stirring evenly, ultrasonically disperse for 25-40 minutes to obtain the first material;
[0029] S2, adding ferric nitrate, manganese nitrate, zinc nitrate and nickel nitrate into water to dissolve to obtain the second material;
[0030] S3, adding the second material dropwise to the first material, followed by evaporating and drying, roasting, and cooling to obtain a powder material;
[0031]S4. Add neodymium oxide, vanadium oxide, niobium oxide, boron oxide, calcium carbonate, lithium carbonate, barium carbonate, silicon dioxide and binder to the powder material for spray granulation, tablet molding, and sintering to obtain low-loss soft powder. Ferrite material.
Embodiment 1
[0034] A kind of low-loss soft magnetic ferrite material proposed by the present invention, its raw material comprises main material and auxiliary material, and wherein main material comprises: iron nitrate 57 parts, manganese nitrate 42 parts, zinc nitrate 9 parts, nickel nitrate 10 parts; Based on the total weight of main materials, the auxiliary materials include: neodymium oxide 300ppm, vanadium oxide 400ppm, niobium oxide 400ppm, boron oxide 700ppm, calcium carbonate 50ppm, lithium carbonate 100ppm, barium carbonate 20ppm, silicon dioxide 800ppm, adhesive 2000ppm, Adsorbent 5×10 6 ppm, emulsifier 300ppm.
[0035] The preparation method of the above-mentioned low-loss soft ferrite material that the present invention also proposes comprises the following steps:
[0036] S1. After adding the adsorbent and emulsifier into the water and stirring evenly, the first material was obtained after ultrasonic dispersion for 25 minutes;
[0037] S2, adding ferric nitrate, manganese n...
Embodiment 2
[0041] A low-loss soft magnetic ferrite material proposed by the present invention, its raw materials include main materials and auxiliary materials, wherein the main materials include 58 parts of iron nitrate, 41 parts of manganese nitrate, 10 parts of zinc nitrate, and 9.4 parts of nickel nitrate in molar parts; Based on the total weight of main materials, the auxiliary materials include: neodymium oxide 320ppm, vanadium oxide 360ppm, niobium oxide 450ppm, boron oxide 600ppm, calcium carbonate 100ppm, lithium carbonate 90ppm, barium carbonate 50ppm, silicon dioxide 600ppm, adhesive 2200ppm, Adsorbent 4×10 6 ppm, emulsifier 350ppm.
[0042] The preparation method of the above-mentioned low-loss soft ferrite material that the present invention also proposes comprises the following steps:
[0043] S1. After adding the adsorbent and emulsifier into water and stirring evenly, the first material was obtained after ultrasonic dispersion for 40 minutes, wherein the weight ratio of ...
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