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Water-soluble anise oil microemulsion for cigarettes and preparation method and application thereof

An anise oil and microemulsion technology, applied in the field of microemulsion, can solve the problems of low scale utilization, large microcapsule particle size, and inability to use, etc., and achieve easy control and measurement, low volatility, and coordinated cigarette aroma Effect

Inactive Publication Date: 2015-11-11
HUBEI CHINA TOBACCO IND +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, traditional microcapsule products usually exist in solid form and cannot be used in liquid food, cosmetics, flavors, and medicines. In addition, due to the large particle size of microcapsules, their large-scale utilization is not very high, and the addition amount is small case, it is also not conducive to achieving a uniform distribution in the product

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] Select polyoxyethylene sorbitan monolaurate and maltitol as the compound emulsifier, and the mass ratio of the two emulsifiers is 1:4; select ethanol as the co-emulsifier, and the mass ratio of the compound emulsifier to the co-emulsifier is 3 :2. Get 1500g of anise oil, the total amount of emulsifier and co-emulsifier is 1500g, promptly get polyoxyethylene sorbitan monolaurate 180g, maltitol 720g, co-emulsifier 600g, and the add-on of water is 2000g.

[0029] After mixing the oil phase and the emulsified phase, use mechanical stirring for 30 minutes, stir and mix evenly, then add the water phase, continue to stir for 30 minutes, and divide and pack them into brown glass bottles according to the required amount, that is, the water-soluble cigarette water-soluble powder of the present invention is prepared. Anise oil microemulsion1.

[0030] After the preparation of the water-soluble anise oil microemulsion 1 sample for tobacco was completed, its stability was further i...

Embodiment 2

[0032] Select polyoxyethylene sorbitan monolaurate and polyoxyethylene sorbitan monostearate as compound emulsifier, the ratio of two kinds of emulsifiers is 1:1, co-emulsifier selects propylene glycol, compound emulsifier and co-emulsifier The ratio of emulsifier is 3:2. Get anise oil 1200g, the total amount of emulsifier and co-emulsifier is 2000g, namely get polyoxyethylene sorbitan monolaurate 600g, polyoxyethylene sorbitan monostearate 600g, co-emulsifier 800g, And the addition of water is 1800g.

[0033] After mixing the oil phase and the emulsified phase, use mechanical stirring for 30 minutes, stir and mix evenly, then add the water phase, continue to stir for 30 minutes, and pack them into brown glass bottles according to the required amount, that is, the water-soluble cigarette water-soluble powder of the present invention is prepared. Anise oil microemulsion2.

[0034] After the preparation of the tobacco water-soluble anise oil microemulsion 2 sample was complete...

Embodiment 3

[0036] Select polyoxyethylene sorbitan monostearate and polyoxyethylene sorbitan monooleate as compound emulsifiers, the ratio of the two emulsifiers is 1:3, co-emulsifier selects glycerin, compound emulsifier The ratio with co-emulsifier is 3:2. Get anise oil 800g, the total amount of emulsifier and co-emulsifier is 1200g, namely get polyoxyethylene sorbitan monostearate 180g, polyoxyethylene sorbitan monooleate 540g, co-emulsifier 480g, The addition of water is 2000g.

[0037] After mixing the oil phase and the emulsified phase, use mechanical stirring for 30 minutes, stir and mix evenly, then add the water phase, continue stirring for 30 minutes, and pack them into brown glass bottles according to the required amount, and then the smoking water of the present invention is obtained. Soluble anise oil microemulsion3.

[0038]After the preparation of the tobacco water-soluble anise oil microemulsion 3 sample was completed, its stability was further investigated. One method ...

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PUM

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Abstract

The invention relates to a water-soluble anise oil microemulsion for cigarettes and a preparation method and an application thereof. The water-soluble anise oil microemulsion for cigarettes is an O / W type microemulsion system that comprises anise oil, composite emulsifier, co emulsifier and water, and the water-soluble anise oil microemulsion for cigarettes can be used for cigarettes added essence blending. The water-soluble anise oil microemulsion for cigarettes improves water solubility, added essence physical state and fragrance stability of the anise oil; the water-soluble anise oil microemulsion for cigarettes can be used to prepare added essence for cigarettes to replace common anise oil and lift fennel fragrance and pungent fragrance characteristics, enrich the cigarettes fragrance and coordinate the cigarettes fragrance. By adopting the water-soluble anise oil microemulsion for cigarettes, no additional equipment for production is required; no production technology shall be changed; anise oil can be solubilized to that the anise oil can be applied in water-soluble products; product quality can be improved; product stability, fragrance characteristics and sense organs breath effect can be lifted; and a new product application method is developed.

Description

technical field [0001] The invention relates to the technical field of microemulsions, in particular to a tobacco water-soluble anise oil microemulsion, a preparation method and application thereof. Background technique [0002] Anise oil, colorless or light yellow liquid, soluble in ethanol and ether, the main component is anethole, so it is a natural raw material for extracting anethole, and it is also used to prepare flavoring agents for beverages, food, tobacco, etc. and medicine. Anise oil is mainly used directly for cooking seasoning, or for extracting essential oils. Aniseed oil is the main raw material for the synthesis of negative hormone hexestrol in medicine. Fennel oil is obtained from the fruit or branches of fennel as raw material by direct steam distillation under normal pressure. The distillate is cooled, clarified, oil-water separated, and vacuum dehydrated to obtain the finished fennel oil. The effluent water is re-distilled, and a small amount of essentia...

Claims

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Application Information

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IPC IPC(8): A24B3/12C08L91/00C08J3/03
Inventor 程书锋杨鑫熊国玺苗丽坤肖龙恩喻世涛
Owner HUBEI CHINA TOBACCO IND
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