LED (light-emitting diode) lamp glass lamp shell heat-conducting and explosion-proof coating material and preparation method thereof
A technology for LED lamps and coating materials, applied in the direction of coating, etc., can solve the problems of volatile solvents, flammable biological toxicity, thermal conductivity not described, shortening the life of the filament, etc., to achieve good compatibility, improve the maintenance of luminous flux efficiency and reduce security risks
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Embodiment 1
[0028] A method for preparing a thermally conductive explosion-proof coating material for a glass lamp housing of an LED lamp, comprising the following steps
[0029] Preparation of modified graphene: add 1 part of graphene oxide to 10 parts of N,N-dimethylformamide, after ultrasonic dispersion, add 1 part of KH-570, stir evenly, heat up to 110°C, and react for 8 hours . After the reaction product was centrifuged and washed four times with methanol, it was vacuum-dried at 50°C to obtain the modified graphene.
[0030] Preparation of component A: Add 0.2 parts of modified graphene to 10 parts of toluene, ultrasonically disperse evenly, then add 100 parts of vinyl silicone oil (vinyl content 0.15%, viscosity 3000cs), put it in a vacuum defoamer and mix evenly . The toluene in the solution was removed using a rotary evaporator to obtain a mixture. Add 0.3 parts of 3000ppm chloroplatinic acid catalyst and mix well to make component A.
[0031] Preparation of component B: 73 pa...
Embodiment 2
[0033] A method for preparing a thermally conductive explosion-proof coating material for a glass lamp housing of an LED lamp, comprising the following steps
[0034] Preparation of modified graphene: Add 1 part of graphene oxide to 10 parts of N,N-dimethylformamide, after ultrasonic dispersion, add 1 part of vinyltrimethoxysilane, stir evenly, heat up to 130 ° C, React for 4 hours. After the reaction product was centrifuged and washed four times with methanol, it was vacuum-dried at 50°C to obtain the modified graphene.
[0035] Preparation of component A: Add 0.4 parts of modified graphene to 10 parts of toluene, ultrasonically disperse evenly, then add 100 parts of methyl vinyl silicone oil (vinyl content 0.25%, viscosity 1000cs), and put it in a vacuum defoamer well mixed. The toluene in the solution was removed using a rotary evaporator to obtain a mixture. Add 0.5 parts of 2000ppm chloroplatinic acid catalyst and mix well to make component A.
[0036] Preparation of ...
Embodiment 3
[0038] A method for preparing a thermally conductive explosion-proof coating material for a glass lamp housing of an LED lamp, comprising the following steps
[0039] Preparation of modified graphene: Add 1 part of graphene oxide to 10 parts of N,N-dimethylformamide, after ultrasonic dispersion, add 1 part of KH-560, stir evenly, heat up to 110°C, and react for 8 hours . After the reaction product was centrifuged and washed four times with methanol, it was vacuum-dried at 50°C to obtain the modified graphene.
[0040] Preparation of component A: Add 0.2 parts of modified graphene to 10 parts of toluene, ultrasonically disperse evenly, then add 100 parts of methyl vinyl silicone oil (vinyl content 0.1%, viscosity 5000cs), and put it in a vacuum defoamer well mixed. The toluene in the solution was removed using a rotary evaporator to obtain a mixture. Add 0.1 part of 5000ppm platinum complex catalyst coordinated by methylvinylsiloxane, mix well, and make A component.
[0041...
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