Preparation method of azotized graphene lithium ion power battery slurry
A technology of graphene nitride and lithium-ion batteries, which is applied in the direction of battery electrodes, circuits, electrical components, etc., can solve the problems of graphene nitride quality reduction, high nitriding treatment temperature, unsuitable for industrial production, etc., to increase the amount of addition , Improve the high temperature cycle and improve the effect of safety
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0037] Step 1. Preparation of pre-nitrided expandable graphite: First, weigh 15 parts of graphite, 10 parts of concentrated sulfuric acid, 30 parts of potassium permanganate, and 5 parts of ammonium bicarbonate in parts by weight, mix them thoroughly, and stir and react at 80°C for 0.5- 2h, after washing, add 10 parts of ammonium bicarbonate, mix evenly, carry out the second pre-nitridation at 120°C, and dry for 3 hours to obtain pre-nitrided expandable graphite;
[0038]Step 2. Preparation of nitrided expanded graphite: the above-mentioned pre-nitrided expandable graphite is treated at a high temperature of 1000° C., and nitriding treatment is carried out during the expansion process to obtain nitrided expanded graphite;
[0039] Step 3. Preparation of graphene nitride lithium-ion power battery slurry (the following parts are all weighed by weight):
[0040] (1) Add 100 parts of N-methylpyrrolidone into the mixer tank, wherein the mixer tank is connected to a cooling cycle, a...
Embodiment 2
[0045] Step 1. Preparation of pre-nitrided expandable graphite: First, weigh 10 parts of graphite, 15 parts of concentrated sulfuric acid, 40 parts of potassium dichromate, and 5 parts of ammonium carbonate in parts by weight, mix them thoroughly, stir and react at 60°C for 2 hours, wash Then add 15 parts of ammonium carbonate, mix evenly, carry out the second step of pre-nitridation at 120°C, and dry for 3 hours to obtain pre-nitrided expandable graphite;
[0046] Step 2. Preparation of nitrided expanded graphite: the pre-nitrided expandable graphite is expanded by microwave, the microwave output power is 1500w, and the time is 2min. During the expansion process, nitriding treatment is carried out at the same time to obtain nitrided expanded graphite;
[0047] Step 3. Preparation of graphene nitride lithium-ion power battery slurry (the following parts are all weighed by weight):
[0048] (1) Add 100 parts of N-methylpyrrolidone into the mixer tank, wherein the mixer tank is ...
Embodiment 3
[0053] Step 1. Preparation of pre-nitrided expandable graphite: First, weigh 20 parts of graphite, 15 parts of potassium permanganate, 20 parts of perchloric acid, and 5 parts of urea in parts by weight, mix them thoroughly, stir and react at 60°C for 2 hours, and then wash Add 10 parts of urea, mix well, carry out the second pre-nitridation at 120°C and dry for 3 hours to obtain pre-nitrided expandable graphite;
[0054] Step 2. Preparation of nitrided expanded graphite: The above-mentioned pre-nitrided expandable graphite is treated at a high temperature of 1000 ° C, that is, the nitriding treatment is carried out during the expansion process, and then the nitrided expanded graphite is passed into the boiling furnace, and the temperature is 800 ° C. , nitrogen purging for post-nitridation treatment, and finally collected to obtain nitrided expanded graphite;
[0055] Step 3. Preparation of graphene nitride lithium-ion power battery slurry (the following parts are all weighed...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com