Method for preparing super-hydrophilic and hydrophobic composite nano array interface material
A nano-array, interface material technology, applied in nanotechnology, metal material coating process, device for coating liquid on surface, etc., can solve problems such as unfavorable unified production standards, industrial application, complex process, etc., and achieve benefits for industrialization. The effect of production, cheap and easy-to-obtain raw materials, and innovative methods
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Embodiment 1
[0025] A method for preparing a super-hydrophobic composite nano-array interface material, comprising the following steps:
[0026] 1) Cut a 4cm×4cm copper sheet as the base material, and polish the copper sheet with 800 mesh, 1500 mesh, and 3000 mesh in turn to make the surface rough. Sonicate in acetone, absolute ethanol, and ultrapure aqueous solution for 5 minutes respectively, take out the nitrogen gas and blow dry, and then place it in a 60°C oven for oxidation for 1 hour to seed the copper-based surface;
[0027] 2) Configure chemical bath solution, select c(Zn 2+ ) : c(OH + ) = molar ratio of 1:8, Zn 2+ is derived from zinc nitrate hexahydrate [Zn(NO 3 ) 2 6H 2 O], OH + The source of NaOH is sodium hydroxide, respectively measure 25mL of the solution in a 40mm×70mL weighing bottle, mix and stir until clear to form a chemical bath solution. Suspend the copper sheet in the chemical bath solution in reverse, and prepare the zinc oxide nanocone film by chemical bath...
Embodiment 2
[0032]A method for preparing a super-hydrophobic composite nano-array interface material, comprising the following steps:
[0033] 1) Cut a 4cm×4cm copper sheet as the base material, polish the copper sheet with 800 mesh, 1500 mesh, and 3000 mesh in turn to make the surface rough, and then ultrasonically in acetone, absolute ethanol, and ultrapure aqueous solution for 5 minutes to remove nitrogen After drying, place it in an oven at 60°C for 2 hours to oxidize to seed the copper-based surface;
[0034] 2) Configure chemical bath solution, select c(Zn 2+ ) : c(OH + ) = molar ratio of 1:8, Zn 2+ is derived from zinc nitrate hexahydrate [Zn(NO 3 ) 2 6H 2 O], OH + The source of sodium hydroxide (NaOH), respectively measure 25mL solution in a 40mm × 70mL weighing bottle, mix and stir until clear to form a chemical bath solution, hang the copper piece in the chemical bath solution in reverse, heat at 60 ° C Zinc oxide nanocone film was prepared by chemical bath deposition at ...
Embodiment 3
[0039] A method for preparing a super-hydrophobic composite nano-array interface material, comprising the following steps:
[0040] 1) Cut a 4cm×4cm copper sheet as the base material, polish the copper sheet with 800 mesh, 1500 mesh, and 3000 mesh in turn to make the surface rough, and ultrasonically in acetone, absolute ethanol, and ultrapure aqueous solution for 5 minutes respectively, and take out nitrogen After drying, place it in an oven at 60°C for 2 hours to oxidize to seed the copper-based surface;
[0041] 2) Configure chemical bath solution, select c(Zn 2+ ) : c(OH + ) = molar ratio of 1:8, Zn 2+ is derived from zinc nitrate hexahydrate [Zn(NO 3 ) 2 6H 2 O], OH + The source of sodium hydroxide (NaOH), respectively measure 25mL solution in a 40mm × 70mL weighing bottle, mix and stir until clear to form a chemical bath solution, hang the copper piece in the chemical bath solution in reverse, heat at 60 ° C Zinc oxide nanocone film was prepared by chemical bath d...
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