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Novel organic silicon defoaming agent with excellent stability and defoaming ability

A technology of silicone defoamer and stability, which is applied in the field of new emulsion type silicone defoamer, which can solve problems such as limitations, difficulty in developing the excellent properties of emulsion, and easy demulsification

Active Publication Date: 2015-05-27
河北华茂环保科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the emulsion is a thermodynamically unstable system. If the emulsification is not complete enough, the emulsion is prone to delamination and demulsification as the storage time increases, making it difficult to exert the excellent properties of the emulsion, thereby reducing its defoaming performance. However, if the emulsion system is too stable, its defoaming ability will decrease
Some products of traditional defoamers have good defoaming performance, but the emulsion is not stable enough, and they are easy to break when used, which limits their use; some products have good stability, but their defoaming performance is poor
Therefore, the traditional emulsion-type defoamer still needs a breakthrough in terms of not affecting the defoaming performance and having better stability.

Method used

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  • Novel organic silicon defoaming agent with excellent stability and defoaming ability

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0006] Embodiment 1: prepare 150g of emulsion type silicone defoamer, its preparation method is:

[0007] 1) Add silicone paste 10% + 3% compound emulsifier into a 250ml beaker (of which: 64% Pingping + 36% C 18 ~C 16 Alcohol)+CMC- HV 0.6%;

[0008] 2) Then use a heater to control a certain temperature (70 ° C ~ 80 ° C) to heat it into a molten state, stir it evenly with a glass rod, stop heating, and cool to room temperature;

[0009] 3) Finally, the defoamer was emulsified by a high-shear emulsifier at a speed of 10,000 r / min for 5 minutes while adding water to obtain the defoamer.

Embodiment 2

[0010] Embodiment 2: prepare 150g of emulsion type silicone defoamer, its preparation method is:

[0011] 1) Add silicone paste 10% + 3% compound emulsifier into a 250ml beaker (of which: 64% Pingping + 36% C 18 ~C 16 Alcohol)+CMC- HV 0.6% + diethylene glycol methyl ether 2%;

[0012] 2) Then use a heater to control a certain temperature (70 ° C ~ 80 ° C) to heat it into a molten state, stir it evenly with a glass rod, stop heating, and cool to room temperature;

[0013] 3) Finally, the defoamer was emulsified by a high-shear emulsifier at a speed of 10,000 r / min for 5 minutes while adding water to obtain the defoamer.

Embodiment 3

[0014] Embodiment 3: prepare 150g of emulsion type silicone defoamer, its preparation method is:

[0015] 1) Add silicone paste 10% + 3% compound emulsifier into a 250ml beaker (of which: 64% Pingping + 36% C 18 ~C 16 Alcohol)+CMC- HV 0.6% + diethylene glycol methyl ether 3%;

[0016] 2) Then use a heater to control a certain temperature (70 ° C ~ 80 ° C) to heat it into a molten state, stir it evenly with a glass rod, stop heating, and cool to room temperature;

[0017] 3) Finally, the defoamer was emulsified by a high-shear emulsifier at a speed of 10,000 r / min for 5 minutes while adding water to obtain the defoamer.

[0018] Performance evaluation:

[0019] 1) Preparation of foaming liquid: Accurately weigh K12 (sodium lauryl sulfate) foaming agent, dissolve it in standard mineralized water (CaCl 2 5.2g / L, MgCl 2 .6H 2 O 3.5g / L, Na 2 SO 4 7.0g / L, NaCl14.3g / L), be made into 0.05% foaming agent mineralized aqueous solution.

[0020] 2) Preparation of defoaming solut...

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Abstract

The invention discloses a method for preparing a novel organic silicon defoaming agent with excellent stability and defoaming ability. The traditional emulsion type defoaming agent is good in defoaming performance and low in stability or is high in stability and poor in defoaming performance. The method disclosed by the invention is characterized in that a certain amount of diethylene glycol monomethyl ether is added during preparation, the defect that the stability and defoaming performance of the traditional emulsion type defoaming agent are difficultly considered simultaneously is overcome, and the stability of the emulsion is greatly improved under the condition that excellent defoaming performance of the defoaming agent is guaranteed. According to the technical scheme, the organic silicon defoaming agent comprises the following four substances in percentage by mass: 10-20 percent of silicone cream, 3-5 percent of a composite emulsifier, 0.6-1 percent of CMC-HV and 2-5 percent of diethylene glycol monomethyl ether, wherein the composite emulsifier comprises 57-72 percent of peregal and 28-43 percent of fatty alcohol, and the HLB value is 9-12. The preparation method comprises the following steps: adding the four substances into a reactor, heating, uniformly stirring, and cooling to room temperature; and finally, and emulsifying at a certain rotating speed for 5 minutes by virtue of a high-shear emulsifying machine while adding water, thereby obtaining the defoaming agent.

Description

technical field [0001] The invention relates to the field of silicone defoamers, and is a novel emulsion type silicone defoamer with excellent stability and defoaming performance. Background technique [0002] Foam will greatly restrict production capacity and reduce production capacity. The existence of foam affects many production processes, and will bring unnecessary pollution to the environment and affect the national economy. Therefore, in some production processes, it is necessary to control the influence of foam on the process. [0003] In recent years, with the expansion of industrial production scale and the strengthening of environmental governance, various defoamers have emerged as the times require, and have developed into a major industry. Among them, the silicone defoamer not only has the effect of instantaneous defoaming, but also has a long-lasting anti-foaming effect, and has the advantages of less dosage, wide application range, and chemical inertness. C...

Claims

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Application Information

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IPC IPC(8): B01D19/04
Inventor 张文杜昱熹姚瑶孔凡波
Owner 河北华茂环保科技有限公司
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