Humidity-sensitive composite membrane, preparation method of humidity-sensitive composite membrane and humidity sensor
A moisture-sensitive composite film and film-forming technology, applied in the field of sensitive materials, can solve the problems of long measurement period (generally more than one week, difficult and cumbersome accurate detection, expensive equipment, etc.)
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Embodiment 1
[0065] The preparation method of moisture-sensitive composite film of the present invention comprises the following steps:
[0066] ① Prepare a mixed solution of poly(4-vinylpyridine) and polyvinyl butyral, the concentration of poly(4-vinylpyridine) is 36 mg / mL, and the concentration of polyvinyl butyral is 5 mg / mL;
[0067] ② Add 1,4-dibromobutane with a molar ratio of 2 times that of poly(4-vinylpyridine), and age for 10 h to form a mixed solution;
[0068] ③ After drying the mixed solution in step ② to form a film, heat at 110°C for 10 h to prepare the first layer of polyelectrolyte membrane;
[0069] ④ Prepare a mixed solution of silver nitrate and polyvinyl alcohol, the concentration of silver nitrate is 0.05mol / L, and the concentration of polyvinyl alcohol is 30mg / mL;
[0070] 5. the mixed solution in step 4. is formed into a film on the polyelectrolyte membrane and dried;
[0071] ⑥ In the glutaraldehyde environment, the in situ reduction cross-linking reaction was ca...
Embodiment 2
[0115] ① Prepare a mixed solution of poly(2-vinylpyridine) and polyvinyl alcohol, the concentration of poly(2-vinylpyridine) is 5 mg / mL, and the concentration of polyvinyl alcohol is 100 mg / mL;
[0116] ② Add 1,5-dibromopentane with a molar ratio of 0.2 times poly(2-vinylpyridine), and age for 48 h to form a mixed solution;
[0117] ③ After drying the mixed solution in step ② to form a film, heat at 40°C for 48 h to prepare the first layer of polyelectrolyte membrane;
[0118] ④ prepare a mixed solution of copper sulfate and polyethylene glycol, the concentration of copper sulfate is 0.005mol / L, and the concentration of polyethylene glycol is 300mg / mL;
[0119] 5. the mixed solution in step 4. is formed into a film on the polyelectrolyte membrane and dried;
[0120] ⑥ Under the environment of adipaldehyde, carry out in situ reductive cross-linking reaction for 48 hours at a temperature of 10°C to prepare a moisture-sensitive composite film.
[0121] The resulting moisture-se...
Embodiment 3
[0123] ① Prepare a mixed solution of poly(4-vinylpyridine) and polyvinylpyrrolidone, the concentration of poly(4-vinylpyridine) is 400 mg / mL, and the concentration of polyvinylpyrrolidone is 0.5 mg / mL;
[0124] ② Add 1,6-dibromohexane with a molar ratio of 15 times poly(4-vinylpyridine), and age for 0.5 h to form a mixed solution;
[0125] ③ After drying the mixed solution in step ② to form a film, heat at 200°C for 0.2 h to prepare the first layer of polyelectrolyte membrane;
[0126] ④ Preparation of chloroauric acid (H[AuCl 4 ]) and polypropylene glycol mixed solution, the concentration of chloroauric acid is 1mol / L, and the concentration of polypropylene glycol is 3mg / mL;
[0127] 5. the mixed solution in step 4. is formed into a film on the polyelectrolyte membrane and dried;
[0128] ⑥ Under the environment of malondialdehyde, the in situ reduction cross-linking reaction was carried out at 200 °C for 0.1 h to prepare the moisture-sensitive composite film.
[0129] The...
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