Rhodamine B-based fluorescence sensor and preparation
A technology of fluorescent sensor and aminocaproic acid, which is applied in the field of fluorescent sensor and its preparation, can solve the problems of expensive detection and insufficient fast detection, and achieve the effects of good selectivity, high sensitivity, and resource saving
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[0022] The synthetic route of the present invention is as follows:
[0023]
[0024] 1. Synthesis of target compounds
[0025] 1. Add 100 mg of 3-(3',6'-bis(diethylamino)-3-oxaspiro[isoindoline-1,-1,9'-xanthene]-2-yl)propane (see the article Design and synthesis of a novel Rhodamine B[2]rotaxane) was dissolved in 5mL of methanol, then 79mg of 6-aminocaproic acid was added, and stirred at room temperature for 2h;
[0026] 2. Weigh 85mg of sodium triacetylborohydride, dissolve it in 1ml of tetrahydrofuran, add it to the above reaction solution with a pipette gun, continue to stir at room temperature, use TLC to detect the reaction progress, and the reaction is complete in 3 hours;
[0027] 3. Add 1 mL of saturated sodium bicarbonate solution dropwise to the above reaction solution, and continue to stir for 10 minutes. The saturated sodium bicarbonate is to quench the sodium triacetylborohydride added thereto;
[0028] 4. Remove the solvent with a rotary evaporator, and sepa...
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