A kind of co-production extraction and separation method of eucommia fine powder, eucommia polysaccharide and eucommia gum
A technology of eucommia fine powder and separation method, which is applied in the direction of medical formula, medical preparations containing active ingredients, plant/algae/fungus/moss components, etc., which can solve the problem of low-cost utilization of eucommia gum and structural changes of eucommia gum , long period of Eucommia gum, etc., to achieve the effect of comprehensive development and utilization, short extraction and separation time, and clear solution
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Embodiment 1
[0039] (1) Pre-treatment steps: After removing impurities, the leaves of Eucommia ulmoides are passed the inspection according to the quality requirements of the Chinese Pharmacopoeia, and exposed to the sun; the dried leaves of Eucommia ulmoides are mechanically crushed to a particle size of 10 mesh, and placed in a dry and cool place for later use .
[0040] (2) Extraction step: mix the eucommia leaves treated in step (1) according to the ratio of solid to liquid 1:20, extract at 60°C for 3 hours, filter the extract, and pump it to the storage tank for the second time When extracting, mix according to the ratio of solid to liquid of 1:5, and the extraction temperature and time are the same as the first time; the solution in the two extraction processes is pure water.
[0041] (3) Tube membrane filtration step: the mixed solution extracted in step (2) is removed and filtered by tube membrane filtration, wherein the tube membrane molecular weight cut-off is 20000D.
[0042] (...
Embodiment 2
[0056] (1) Pre-treatment step: After removing impurities, the leaves of Eucommia ulmoides are passed the inspection according to the quality requirements of the Chinese Pharmacopoeia, and exposed to the sun; the dried leaves of Eucommia ulmoides are mechanically crushed to 18 meshes, and placed in a dry and cool place for later use.
[0057] (2) Extraction step: mix Eucommia leaves treated in step (1) according to the ratio of solid to liquid ratio of 1:10, extract at 65°C for 2.5h, filter the extract, and pump it to the liquid storage tank for two During the second extraction, mix according to the ratio of solid to liquid of 1:10, and the extraction temperature and time are the same as the first time; the solution is pure water during the two extractions.
[0058] (3) Tube membrane filtration step: the mixed solution extracted in step (2) is removed and filtered by tube membrane filtration, wherein the tube membrane molecular weight cut-off is 25000D.
[0059] (4) Finished pr...
Embodiment 3
[0073](1) Pre-treatment steps: After removing impurities, the dried bark of Eucommia is passed the inspection according to the quality requirements of the Chinese Pharmacopoeia, and exposed to the sun; the dried bark of Eucommia is mechanically crushed to 20 meshes, and placed in a dry and cool place spare.
[0074] (2) Extraction step: mix the bark of Eucommia ulmoides treated in step (1) according to the ratio of material to liquid ratio of 1:15, extract at 70°C for 2 hours, filter the extract, and pump it to the liquid storage tank for the second time When extracting, mix according to the ratio of solid to liquid of 1:15, and the extraction temperature and time are the same as the first time; the solution is pure water during the two extraction processes.
[0075] (3) Tube membrane filtration step: the mixed solution extracted in step (2) is removed and filtered by tube membrane filtration, wherein the tube membrane molecular weight cut-off is 30000D.
[0076] (4) Finished...
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