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Method for preparing pomegranate seed oil rich in vitamin E

A technology for pomegranate seed oil and vitamins, which is applied in the direction of producing fat, fat oil/fat production, etc., can solve the problems of not involving the extraction and protection of the antioxidant component vitamin E, not being able to well inhibit oxidation, and affecting the naturalness of oils and fats, etc. Widely used value, improving punicic acid content and oil yield, not easy to oxidize and deteriorate

Inactive Publication Date: 2014-12-10
SHANXI UNIV OF CHINESE MEDICINE
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  • Summary
  • Abstract
  • Description
  • Claims
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Problems solved by technology

[0006] Chinese patents "A method of producing high-purity punicic acid" (CN100344601C) and "Preparation method of pomegranate seed oil with high content of conjugated unsaturated trienoic acid" (CN100510041C) purify pomegranate through supercritical extraction, rectification and separation steps acid and impurity removal to obtain high-purity punicic acid, but they only focused on the purification of the main component punicic acid, and did not involve the extraction and protection of antioxidant vitamin E
201310045191.9 Magnetic field assisted supercritical CO 2 The method of extracting sunflower seed oil removes the impurities in the sunflower seeds, then mechanically crushes them, and then sieves and classifies them to obtain sunflower seed powder; mixes VE evenly into the pretreated sunflower seed powder, and then puts it in a magnetic field for processing , wherein the magnetic field treatment temperature is 48-52°C, the magnetic field strength is 7800-8200Gs, and the magnetization time is 13-15min; the above-mentioned patent points out that adding a certain amount of VE before extraction can resist oxidation and reduce the acid value, but because pomegranate seeds The oil contains a large amount of conjugated trienoic acid, which is different from linoleic acid in sunflower oil. It is particularly easy to oxidize during processing. The large amount of VE will affect the naturalness of the oil, and its function is single, and the inhibitory effect is limited, so simple Adding VE does not inhibit oxidation well

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  • Method for preparing pomegranate seed oil rich in vitamin E

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] Example 1: 200g of pomegranate seeds were added with anti-oxidant protection agent: 1g of vitamin C, 1g of water-soluble tea polyphenols and 0.06g of vitamin E, after being crushed, sieved through a 10-mesh sieve, dried at 40°C for 4 hours, and added to the extraction kettle , adjust the extraction pressure to 28MPa, temperature to 55°C, flow rate to 15L / h, separation temperature to 50°C, separation pressure to 18MPa, and extraction for 3.5 hours. The separated carbon dioxide is liquefied and returned to the storage tank, and then recycled after being pressurized and heated. Isolate pomegranate seed oil 16g, its appearance is transparent and light in color. After analysis and detection, the content of punicic acid in the oil is 81%, the content of vitamin E is 200mg / 100g, the acid value is 2.5mgKOH / g, and the peroxide value is 0.08%.

Embodiment 2

[0021] Example 2: 200g of pomegranate seeds were added with anti-oxidant protection agent: 2g of vitamin C, 5g of fat-soluble tea polyphenols and 0.3g of vitamin E, after being crushed, sieved through a 40-mesh sieve, dried at 25°C for 6 hours, and then added to the extraction kettle , adjust the supercritical extraction separation parameters as in Example 1, and extract for 2.5 hours. 11g of pomegranate seed oil was isolated, and its appearance was transparent and light in color. After analysis and detection, the content of punicic acid in the oil is 83%, the content of vitamin E is 660mg / 100g, the acid value is 1.2 mgKOH / g, and the peroxide value is 0.02%.

Embodiment 3

[0022] Example 3: 200g of pomegranate seeds were added with anti-oxidant protection agent: 4g of vitamin C, 2g of fat-soluble tea polyphenols and 0.1g of vitamin E, after being crushed, sieved through a 20 mesh, dried at 85°C for 2 hours, and then added to the extraction kettle , adjust the extraction parameters: pressure 30MPa, temperature 45°C, flow rate 10L / h, separation temperature 40°C, separation pressure 10MPa, extraction for 3 hours. Isolate 28g of pomegranate seed oil, its appearance is transparent and light in color. After analysis and detection, the content of punicic acid in the oil is 85%, the content of vitamin E is 420mg / 100g, the acid value is 1.2mgKOH / g, and the peroxide value is 0.03%.

[0023] For the preparation method listed in the above-mentioned examples 1, 2, and 3, except the listed parameters for supercritical carbon dioxide extraction and separation, each parameter can be selected within the following ranges: extraction pressure 16-40MPa, extraction ...

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Abstract

The invention belongs to the technical field of pomegranate seed oil extraction, and aims at providing a method for preparing pomegranate seed oil rich in vitamin E. the pomegranate seed oil prepared by using the method is high in oil oxidation resistance and high in quality and can be used in medical cosmetics. The method comprises the following steps: firstly, adding a certain amount of vitamin C, tea polyphenol and vitamin E for anti-oxidation protection into pomegranate seeds, crushing pomegranate seeds, heating and drying to make pomegranate seed powder; secondly, extracting the pomegranate seed powder by using a supercritical carbon dioxide solvent, thereby obtaining the pomegranate seed oil rich in vitamin E. Due to addition of tea polyphenol and vitamin E in pretreatment before extraction, the punicic acid and the rich vitamin E in the pomegranate seeds can be protected, and thus the pomegranate seed oil rich in punicic acid and vitamin E is prepared. The pomegranate seed oil prepared by using the method is high in nutrient component content and high in oxidation resistance, can solve the problems that the pomegranate seed oil is easy to deteriorate because of oxidation and is poor in stability, and can be used in the medical cosmetic industry.

Description

technical field [0001] The invention belongs to the technical field of pomegranate seed oil extraction, and in particular relates to a preparation method of pomegranate seed oil rich in vitamin E. Background technique [0002] In daily life, some unfavorable factors such as unhealthy diet, frequent exposure to the sun, stress, environmental pollution, etc., make our living organisms be threatened by free radical oxidation everywhere. Free radicals are indispensable particles in the metabolic activities of life, but excessive free radicals will decompose cells and tissues through oxidation, affect metabolic functions, and cause degenerative changes in the body. In mild cases, oxidation phenomena such as dull complexion and water shortage will occur Seriously, it will cause different health problems, such as common arteriosclerosis, diabetes, cataract, cardiovascular disease, Alzheimer's disease, arthritis, cancer, etc. Therefore, we should take in enough antioxidants to remov...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B1/04C11B1/10
Inventor 杜俊民张朔生孟祥龙孙琳李坤马俊楠王明芳
Owner SHANXI UNIV OF CHINESE MEDICINE
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