Wood modifier and preparation method thereof
A modifier and wood technology, applied in the direction of wood impregnation, wood impregnation, wood processing appliances, etc., can solve the problems of easy cracking and deformation of wood, and achieve the effects of high retention rate, simple process and obvious performance improvement.
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Embodiment 1
[0045] Synthesis of low molecular weight phenolic resin:
[0046] By weight, first add the first batch of materials, 120 parts of phenol and 200 parts of formaldehyde solution, heat up to make the reaction temperature to 40 ° C; then add the first batch of 5 parts of aqueous sodium hydroxide solution with a mass ratio of 40%, continue heating, when Stop heating when the reaction temperature reaches 50°C, and strictly control the reaction temperature at 85-88°C; Two batches of 45 parts of formaldehyde solution, keep the temperature at 75-85°C for 3 hours, cool down to 60°C, add 40 parts of urea, react for half an hour, then gradually lower the temperature to 40°C to obtain low molecular weight phenolic resin.
[0047] Synthesis of flame retardants:
[0048] By weight, first add 1,800 parts of water, 200 parts of ammonia water, 450 parts of formaldehyde, and 1,575 parts of dicyandiamide, and add 1,600 parts of phosphoric acid within 40 to 50 minutes after heating up to 65-75°C,...
Embodiment 2
[0051] Synthesis of low molecular weight phenolic resin:
[0052] By weight, first add the first batch of materials, 150 parts of phenol and 230 parts of formaldehyde solution, heat up to make the reaction temperature to 40 ° C; then add the first batch of 8 parts of aqueous sodium hydroxide solution with a mass ratio of 40%, continue heating, when Stop heating when the reaction temperature reaches 50°C, and strictly control the reaction temperature at 85-88°C; after reacting for 1-1.5 hours, lower the temperature below 70°C, add 12 parts of the second batch of sodium hydroxide solution, and then add Add 25 parts of the second batch of formaldehyde solution, keep the temperature at 75-85°C for 2-3 hours, cool down to 60°C, react for half an hour, then gradually lower the temperature to 40°C to obtain low molecular weight phenolic resin.
[0053] Synthesis of flame retardants:
[0054]By weight, first add 2,000 parts of water, 100 parts of ammonia water, 480 parts of formaldeh...
Embodiment 3
[0057] Synthesis of low molecular weight phenolic resin:
[0058] By weight, first add the first batch of materials, 200 parts of phenol and 300 parts of formaldehyde solution, heat up to make the reaction temperature to 40 ° C; then add the first batch of 10 parts of aqueous sodium hydroxide solution with a mass ratio of 40%, continue heating, when Stop heating when the reaction temperature reaches 50°C, and strictly control the reaction temperature at 85-88°C; after 1-1.5 hours of reaction, lower the temperature below 70°C, add 8 parts of the second batch of sodium hydroxide solution, and then Add 90 parts of the second batch of formaldehyde solution, keep the temperature at 75-85°C for 2-3 hours, cool down to 60°C, add 65 parts of urea, react for half an hour, and then gradually lower the temperature to 40°C to obtain a low molecular weight phenolic resin.
[0059] Synthesis of flame retardants:
[0060] By weight, first add 1900 parts of water, 180 parts of ammonia water,...
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