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Method for dyeing pure cotton black yarns resistant to post-mercerizing strong base

A dyeing method and yarn technology, which is applied in the dyeing field of pure cotton black yarn, can solve the problems of high dye content and COD value, inability to withstand post-mercerizing strong alkali, and difficult wastewater treatment, etc., and achieve good dye promotion rate, The effect of less dye consumption and excellent dye compatibility

Active Publication Date: 2014-10-08
ANHUI HUAMAO TEXTILE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Due to the structural characteristics of this kind of dyes, most of the active groups are bis-chloro-s-triazine structure, which determines its alkali resistance, but the promotion rate is poor and the dyeing rate is low.
At present, all dye manufacturers do not have this type of black dye. Dyeing companies use high-temperature yellow, navy blue, and red color matching when dyeing black. The amount of dye is large, and the weight of dye to the fabric is more than 10% owf. The dyeing rate is low, the dye content and COD value in the waste liquid after dyeing are high, and the wastewater treatment is difficult; the dyeing temperature is as high as 80°C, and the energy consumption is large, so the dyeing cost is high
Although the general traditional medium-temperature reactive black dyes have good promotion rate, high dyeing rate, and low dyeing temperature of 60°C, most of them are composed of C.I. C.I. 82 orange with oxazine active group structure is blended, it is not alkali resistant, so the fabric woven from pure cotton black yarn dyed with this type of reactive dye cannot withstand strong alkali treatment after mercerizing

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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  • Method for dyeing pure cotton black yarns resistant to post-mercerizing strong base

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] Example 1: Black yarn with partial orange light

[0023] The pure cotton yarn was pretreated by conventional one-step descouring and bleaching pretreatment process. Put the pre-treated pure cotton yarn in the large liquid flow skein dyeing vat in the cabinet, close and tighten the dyeing vat door, fill it with soft water, add 0.5g / L sodium hexametaphosphate into the self-expanding vat when the temperature rises to 40°C, Raise the temperature to 50°C; use 3.0% owf reactive black G dye as the main dye, mix with 0.2% owf reactive red S-3B dye, 0.8% owf reactive yellow TS-3R dye, and mix uniformly to make a reactive dye solution. The ratio is 1:10; add the prepared dye solution evenly within 20 minutes, control the heating rate of 1°C / min to 60°C, keep warm for 15 minutes, manually add 80g / L yuan evenly in the self-expanding cylinder within 20 minutes Mingfen, keep warm for 30 minutes, add 20g / L soda ash from the chemical material tank within 30 minutes, keep warm for 75 m...

Embodiment 2

[0024] Example 2: Black yarn with partial purple light

[0025]The pure cotton yarn was pretreated by conventional one-step descouring and bleaching pretreatment process. Put the pre-treated pure cotton yarn in the large liquid flow skein dyeing vat in the cabinet, close and tighten the dyeing vat door, fill it with soft water, add 0.5g / L sodium hexametaphosphate into the self-expanding vat when the temperature rises to 40°C, Raise the temperature to 50°C; use 6% owf reactive black G dye as the main dye, mix with 1% owf reactive red S-3B dye, 0.2% owf reactive navy blue S-G dye, and mix evenly to prepare a reactive dye solution. The dyeing bath ratio is 1 : 20; within 20 minutes, evenly add the prepared dye solution, control the heating rate of 1 ℃ / min to 60 ℃, keep warm for 15 minutes, and manually add 80g / L yuanming powder evenly in the self-expanding cylinder within 20 minutes , keep warm for 30 minutes, add 20g / L soda ash from the chemical material tank within 30 minute...

Embodiment 3

[0026] Example three: black yarn with partial green light

[0027] The pure cotton yarn was pretreated by conventional one-step descouring and bleaching pretreatment process. Put the pre-treated pure cotton yarn in the large liquid flow skein dyeing vat in the cabinet, close and tighten the dyeing vat door, fill it with soft water, add 0.5g / L sodium hexametaphosphate into the self-expanding vat when the temperature rises to 40°C, Raise the temperature to 50°C; use 4.5% owf reactive black G dye as the main dye, mix with 0.3% owf reactive yellow TS-3R dye, 0.5% owf reactive navy blue S-G dye, and mix evenly to prepare a reactive dye solution. The dyeing bath ratio is 1 : 15; within 20 minutes, evenly add the prepared dyeing solution, control the heating rate of 1 ° C / min to 60 ° C, keep warm for 15 minutes, and manually add 80 g / L Yuanming powder evenly within 20 minutes from the expansion tank , keep warm for 30 minutes, add 20g / L soda ash from the chemical material tank wit...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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PUM

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Abstract

The invention discloses a method for dyeing pure cotton black yarns resistant to post-mercerizing strong base. The method comprises the following process steps: preparing a dyeing solution, dyeing, soaping twice, rinsing with hot water for three times, pickling, softening and squeezing water and drying. High-temperature reactive dyes are replaced by medium-temperature reactive dyes in a multiple-active group structure, the dye improvement rate is high, the color yield is high, and the compatibility of the dyes is excellent. Moreover, the dyeing temperature is low, the amount of the dyes is small, the dyeing cost is reduced, the alkali-resistant color fastness of the yarns is greatly improved after the dyed pure cotton black yarns are washed by a soaping solution containing a dispersing agent N, the post-mercerizing strong base resistance of the yarns is high after the yarns are subjected to color fixing through a reactive color fixing agent OS, and the yarns have high application value in actual production. After the yarns are dyed by the dyeing method, the alkali-resistant color fastness of the pure cotton black yarns reaches 4th-5th level, the staining fastness of the yarns reaches the 4th level, and the alkali-resistant fastness index of the colored yarns meets the standard requirement of China.

Description

technical field [0001] The invention relates to a dyeing method of mercerized colored yarn, in particular to a dyeing method of pure cotton black yarn resistant to post-mercerized strong alkali. Background technique [0002] The pure cotton high-count yarn is processed by singeing, mercerizing, dyeing, etc., to make silk-like bright luster, soft and wrinkle-resistant high-quality mercerized dyed yarn. The knitted fabric woven with this yarn is then processed twice After processing such as singeing, post-mercerizing, and softening, it becomes a high-grade pure cotton mercerized fabric. This "double silk double burning" pure cotton mercerized fabric not only fully retains the excellent natural characteristics of raw cotton fiber, but also has silky luster, soft hand feeling, good moisture absorption and breathability, full elasticity and drapability; plus Rich colors, comfortable and casual to wear, fully reflects the temperament and taste of the wearer. With the continuous ...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06P1/38D06P1/673D06P3/66D06P5/02D06P5/04
Inventor 方长国杨蓓章军
Owner ANHUI HUAMAO TEXTILE
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