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Floatation separation method for pyrophyllite and quartz

A separation method and pyrophyllite technology, which are applied in flotation, solid separation and other directions, can solve the problems of complex process structure, high production cost, and many types and dosages of chemicals, and achieve simple process structure, less energy consumption, and less chemicals. Low dosage effect

Active Publication Date: 2014-10-01
XI'AN UNIVERSITY OF ARCHITECTURE AND TECHNOLOGY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] In the flotation separation process of pyrophyllite, quartz and carbonate gangue minerals, since pyrophyllite and quartz are silicon-containing minerals, their buoyancy is close to that of separation; Impurity minerals such as salt are easy to muddy and affect the surface flotation performance of pyrophyllite, which makes it difficult to separate pyrophyllite from gangue minerals such as quartz and carbonate; The development and utilization of pyrophyllite are limited by factors such as the variety and dosage of agents, and the high production cost.

Method used

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  • Floatation separation method for pyrophyllite and quartz
  • Floatation separation method for pyrophyllite and quartz
  • Floatation separation method for pyrophyllite and quartz

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] 1. Mineral raw materials:

[0018] The pyrophyllite content in the mineral raw materials used is 50.11%, the silicon content is 38.45%, and the calcium carbonate content is 13.41%. Phase analysis shows that, except pyrophyllite, silicon-containing minerals mainly exist in the form of silicon dioxide and calcium silicate, and impurity minerals are carbonates and a small amount of muddy minerals.

[0019] 2. Flotation agents and operating conditions:

[0020]

[0021] When in use, the medicament is first prepared into the following weight percent concentrations:

[0022]

[0023]

[0024] Such as figure 1 As shown, during the flotation process, sulfuric acid is used to adjust the pH value of the pulp to 4-5, water glass and sodium hexametaphosphate are added as quartz and gangue mineral inhibitors, and then mixed amine and oxidized paraffin soap are added to trap pyrophyllite. receive. The test shows that the pyrophyllite can be recovered effectively by adopt...

Embodiment 2

[0026] 1. Mineral raw materials:

[0027] The content of pyrophyllite in the mineral raw materials used is 55.37%, the content of silicon is 36.24%, and the content of calcium carbonate is 15.61%. Phase analysis shows that, except for pyrophyllite, silicon-containing minerals mainly exist in the form of silicon dioxide and calcium silicate. The impurity minerals are carbonates and a small amount of muddy minerals.

[0028] 2. Flotation agents and operating conditions:

[0029]

[0030] When in use, the medicament is first prepared into the following weight percent concentrations:

[0031]

[0032] Such as figure 1 As shown, during the flotation process, sulfuric acid is used to adjust the pH value of the pulp to 4-5, water glass and sodium hexametaphosphate are added as quartz and gangue mineral inhibitors, and then mixed amine and oxidized paraffin soap are added to trap pyrophyllite. receive. The test shows that the pyrophyllite can be recovered effectively by adop...

Embodiment 3

[0034] 1. Mineral raw materials:

[0035] The pyrophyllite content in the mineral raw materials used is 58.67%, the silicon content is 40.25%, and the calcium carbonate content is 16.18%. Phase analysis shows that, except for pyrophyllite, silicon-containing minerals mainly exist in the form of silicon dioxide and calcium silicate. The impurity minerals are carbonates and a small amount of muddy minerals.

[0036] 2. Flotation agents and operating conditions:

[0037]

[0038] When in use, the medicament is first prepared into the following weight percent concentrations:

[0039]

[0040] Such as figure 1 As shown, during the flotation process, sulfuric acid is used to adjust the pH value of the pulp to 4-5, water glass and sodium hexametaphosphate are added as quartz and gangue mineral inhibitors, and then mixed amine and oxidized paraffin soap are added to trap pyrophyllite. receive. The test shows that the pyrophyllite can be recovered effectively by using the abo...

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Abstract

The invention discloses a floatation separation method for pyrophyllite and quartz. The method comprises the following steps: in a floatation process, regulating the pH value of ore pulp to 4-5 by using sulfuric acid; adding water glass and sodium hexametaphosphate for serving as quartz and gangue mineral inhibitors; adding mixed amine and oxyparaffin soap for floating pyrophyllite to obtain agalmatolite concentrate. By adopting the method, floatation separation of pyrophyllite and quartz from carbonate gangue mineral can be effectively realized. The agalmatolite concentrate of which the pyrophyllite content is 84.33-86.25 percent and the recovery rate is 78.91-85.24 percent is obtained by performing once rough concentration, three times of scavenging and four times of concentration under the condition that the pyrophyllite content is 50.11-58.67 percent.

Description

technical field [0001] The invention relates to a mineral flotation separation method, in particular to a flotation separation method of pyrophyllite and quartz. Background technique [0002] In the flotation separation process of pyrophyllite, quartz and carbonate gangue minerals, since pyrophyllite and quartz are silicon-containing minerals, their buoyancy is close to that of separation; Impurity minerals such as salt are easy to muddy and affect the surface flotation performance of pyrophyllite, which makes it difficult to separate pyrophyllite from gangue minerals such as quartz and carbonate; The development and utilization of pyrophyllite are limited by factors such as many types and dosages of agents, and high production costs. Contents of the invention [0003] In order to overcome the above-mentioned shortcoming of prior art, the object of the present invention is to provide a kind of flotation separation method of pyrophyllite and quartz, can reclaim pyrophyllit...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B03D1/00B03D1/018
Inventor 卜显忠高珂龙涛张崇辉
Owner XI'AN UNIVERSITY OF ARCHITECTURE AND TECHNOLOGY
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