Preparation method of magnetic bacteria cellulose aerogel oil absorption material
A technology of cellulose airgel and bacterial cellulose, applied in chemical instruments and methods, other chemical processes, fermentation, etc., can solve the problems of human interference, collection difficulties, economic losses and other problems in aquatic ecosystems, and achieve excellent recyclability and selectivity, high oil absorption efficiency, and regular microstructure
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specific Embodiment approach 1
[0029] Specific Embodiment 1: In this embodiment, bacterial cellulose airgel is prepared by dissolving bacterial cellulose microfibrils to form bacterial cellulose hydrogel, and then the bacterial cellulose airgel is modified to produce ultra-light, refractory carbon Nanofiber (CNF) airgel, and finally magnetically modify the CNF airgel by hydrothermal method, so as to be used as an oil-absorbing material for marine oil spills, the specific operation steps are as follows:
[0030] 1. Bacterial cellulose cultivation
[0031] (1) Kombucha liquid subculture medium: the medium is composed of agar, the carbon source is glucose, the nitrogen source is yeast powder and tryptone; the ratio is glucose 5g, yeast powder 1g, agar 2g, CaCO 3 2 g, 100 ml deionized water, and adjust the pH of the medium to 6.8. Scrub the large-mouth glass bottle twice with alcohol, and then boil it in boiling water for two minutes to remove as much bacteria and cleaning agent alcohol as possible to pr...
specific Embodiment approach 2
[0042] Specific implementation mode 2: In this implementation mode, magnetic carbon nanofiber (CNF) airgel oil-absorbing material is prepared according to the following steps:
[0043] 1. Bacterial cellulose cultivation
[0044] (1) Kombucha liquid subculture medium: the medium is composed of agar, the carbon source is glucose, the nitrogen source is yeast powder and tryptone; the ratio is glucose 5g, yeast powder 1g, agar 2g, CaCO 3 2 g, 100 ml of deionized water, and adjust the pH of the medium to 7.0. Scrub the large-mouth glass bottle twice with alcohol, and then boil it in boiling water for two minutes to remove as much bacteria and cleaning agent alcohol as possible to prevent Acetobacter xylinum from being polluted.
[0045] (2) Kombucha was subcultured with bacterial liquid, and an appropriate amount of bacterial liquid was taken from the kombucha liquid (purchased from Yijun Shijia), and inoculated into 100mL fermentation medium with a 20% inoculation amount...
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