Method for detecting Szechuan lovage rhizome
A detection method, the technology of Chuanxiong, applied in the direction of measuring devices, instruments, scientific instruments, etc., can solve the problems of poor specificity, difficult to distinguish, unsuitable index components, etc., and achieve the effect of quality assurance
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Embodiment 1
[0040] Embodiment 1 Detection method of the present invention
[0041] (1) Take about 1.0g of the fine powder of each Rhizoma Chuanxiong sample, weigh it accurately, put it into a stoppered conical flask, add 20ml of ethanol precisely, seal it tightly, and ultrasonically treat it for 40min, filter it, concentrate the filtrate to a 5ml volumetric flask, that is have to.
[0042] (2) Precisely measure 20 μL of the test solution, inject it into a high-performance liquid chromatograph, and detect it at 280 nm. The chromatographic conditions are as follows:
[0043]
[0044] Under the above detection method, multiple common peaks can be separated, and the separation degree of each peak is good, which provides convenience for determining the content of each index component and comparing the similarity of fingerprints. Using the above method to detect medicinal materials of different varieties or textures can not only effectively distinguish the similar varieties of Rhizoma Chuan...
Embodiment 2
[0045] Embodiment 2 The investigation of fingerprint spectrum detection method of the present invention
[0046] ① The preparation method of the test solution was investigated using ethanol as the extraction solvent, and the influence of ultrasonic extraction for 30 minutes and reflux extraction (extracting twice, the first time for 1.5 hours, and the second time for 1 hour) on the chromatographic peak area was investigated. The results showed that ultrasonic extraction Compared with extraction and reflux extraction, the chromatograms are not much different, so the simpler ultrasonic extraction method is chosen. On this basis, the effects of ethanol and methanol on the chromatographic peaks were compared, and the results showed that the number of chromatographic peaks in the ethanol extract was significantly more than that in the methanol extract, so the extraction solvent was determined to be ethanol. The above studies determine that the preparation method of the test solutio...
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