A kind of oil-based liquefied fracturing fluid thickener and preparation method thereof
A fracturing fluid thickener and liquefaction technology, which is applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve the problem of increasing the cleaning and treatment costs of liquid storage tanks, increasing the difficulty of fracturing fluid quality control, and increasing manpower and material resources Consumption and other issues, to achieve the effect of reducing manpower and material resources input, easy quality control, and convenient preparation
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preparation example Construction
[0062] Specifically, the preparation method of the oil-based liquid thickener of the present invention comprises the following steps:
[0063] The first step: the compounding of oil-based organic solvent
[0064]Keep the temperature in the kettle at 10-40°C, add fuel oil organic solvents (including but not limited to one or more of gasoline, diesel, kerosene) or mineral oil organic solvents (including but not limited to One or both of mineral oil and liquid paraffin) or silicone oil organic solvents (including but not limited to one or more of methyl silicone oil, ethyl silicone oil, methyl hydrogen silicone oil, phenyl silicone oil, methyl hydroxy silicone oil ) or vegetable oil organic solvent (including but not limited to one or more of rapeseed oil, corn oil, soybean oil, peanut oil, cottonseed oil), density regulator (dichloromethane, chloroform, carbon tetrachloride , one or more of chlorinated paraffin), performance modifier (one or more of nano-bentonite, polyamide wa...
Embodiment 1
[0074] Preparation and performance test of liquid thickener 1:
[0075] 1) Weigh 58g of gasoline and 57.5g of diesel oil in the kettle and keep stirring; add 21g of dichloromethane and 21.9g of chloroform and stir for 15min; add 6.6g of nano-bentonite and stir for 20min to obtain a compound oil-based organic solvent.
[0076] 2) Keep stirring, add 135 g of hydroxypropyl modified guar gum, and stir for 30 minutes to obtain liquefied thickener 1.
[0077] The product in this embodiment is an emulsion dispersion, and after testing, the density is 1.05g / cm 3 , the gelling time is 20s, and the viscosity of 1.2% liquefied thickener after dissolving is 45mPa.s.
Embodiment 2
[0079] Preparation and performance test of liquid thickener 2:
[0080] 1) Weigh 41g of liquid paraffin and 40g of methyl silicone oil in the kettle and keep stirring; add 7.2g of carbon tetrachloride and stir for 10min; add 0.9g of nano-bentonite and 0.9g of polyamide wax and stir for 25min to obtain the compounded Oil-based organic solvent.
[0081] 2) Keep stirring, add 60g of zwitterionic polyacrylamide and stir for 25min to obtain liquefied thickener 2.
[0082] The product in this embodiment is an emulsion dispersion, and after testing, the density is 1.10g / cm 3 , The gelling time is 20s, and the viscosity of 1.2% liquefied thickener after dissolving is 42mPa.s.
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