Method of infiltrating metal infiltrating agent to cerium-containing neodymium iron boron magnetic material
A magnetic material, NdFeB technology, applied in the direction of magnetic materials, magnetic objects, inorganic materials, etc., can solve the problems of poor comprehensive performance of magnets, large amount of heavy rare earth, low coercive force of NdFeB, etc., to improve the coercivity Effects of coercive force, high coercive force and corrosion resistance
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Embodiment 1
[0026] Using the dual main phase alloy method, the first main phase is broken by hydrogen, and the Nd with a particle size of 0.35 μm is ground by airflow 30 Fe bal B 1 tm 0.8 , and the mass percentage is 20%.
[0027] Using a thickness of 0.3mm (Ce 0.8 Nd 0.2 ) 30 Fe bal B 1 tm 0.8 Quick-setting tablets, Dy with a particle size of less than 2 μm 80 al 20 For metal penetration agent. Dy 80 al 20 The metallization agent and (Ce 0.8 Nd 0.2 ) 30 Fe bal B 1 tm 0.8 Mix evenly, place in a vacuum furnace, and evacuate to 10 -2 Preheat with low power when the Pa is above, and wait until the vacuum reaches 10 again. -2 Pa above, increase the power to raise the temperature to about 650°C, and wait until the vacuum degree is stable at 10 -2 After the Pa is above, fill high-purity hydrogen to -0.06MPa; increase the power and keep the temperature at 800°C for 6 hours, while maintaining the vacuum in the furnace at -0.04MPa, carry out dysprosium and aluminum infiltratio...
Embodiment 2
[0033] Using the dual main phase alloy method, the first main phase is broken by hydrogen, and the Nd with a particle size of 0.30 μm is ground by airflow 30 Fe bal B 1 tm 0.8 , the mass percentage is 40%;
[0034] Using a thickness of 0.3mm (Ce 0.6 Nd 0.4 ) 30 Fe bal B 1 tm 0.8 (wt%) quick-setting tablets, Dy with a particle size of less than 2 μm 91 al 9 For metal penetration agent. The Dy 91 al 9 The metallization agent and (Ce 0.6 Nd 0.4 ) 30 Fe bal B 1 tm 0.8 (wt%) mix homogeneously, place in the vacuum furnace, vacuum up to 10 -2 Preheat with low power when the Pa is above, and wait until the vacuum reaches 10 again. -2 Pa above, increase the power to raise the temperature to about 600°C, and wait until the vacuum degree is stable at 10 -2 After pa is above, fill in H 2 Mixed gas with argon to -0.06MPa; increase the power and keep the temperature at 880°C for 4 hours, while maintaining the vacuum in the furnace at -0.04MPa, carry out infiltration of...
Embodiment 3
[0040] Using the dual main phase alloy method, the first main phase is broken by hydrogen, and the Nd with a particle size of 0.35 μm is ground by airflow 30 Fe bal B 1 tm 0.8 , the mass percentage content is 50%;
[0041] Using a thickness of 0.35mm (Ce 0.5 Nd 0.5 ) 30 Fe bal B 1 tm 0.8 (wt%) quick-setting tablets, Dy with a particle size of less than 2 μm 80 al 10 Cu 10 For metal penetration agent. Mix the metallizing agent and the cerium-containing NdFeB quick-setting sheet with a weight ratio of 3% and mix them evenly, place them in a vacuum furnace, and evacuate them to 10 -2 Preheat with low power when Pa is above, and wait until the vacuum degree is stable at 10 -2 After pa above, raise the power to about 550°C, fill high-purity argon to -0.07MPa; increase the power to keep the temperature at 780°C for 10 hours, while maintaining the vacuum in the furnace at -0.04MPa, carry out dysprosium infiltration and Aluminum, after being broken by hydrogen, is jet-mi...
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