Flame-retardant ceramic composite material and preparation method thereof
A composite material and ceramic technology, applied in the polymer field, can solve the problems of shedding, brittle mica tapes, and high production costs, and achieve the effects of good flexibility and elasticity, isolation from external flames, and low production costs.
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[0074] There are two preparation methods for the flame-retardant ceramic composite material of this embodiment, and the first preparation method includes the following steps:
[0075] ① 100 parts of the polyolefin, 0-100 parts of silicone rubber, 1-100 parts of silicon dioxide, 0-30 parts of silicone oil, 0.00001-10 parts of platinum complex and / or platinum compound calculated as platinum, coupling agent 0-10 parts, 0-10 parts of antioxidant, 1-100 parts of flame retardant are kneaded in a kneader;
[0076] ② Vacuumize the kneader, keep the vacuum at -0.1~-0.04Mpa, and keep the temperature at 100~200°C;
[0077] ③Put 1-250 parts of vitrified powder into the kneader to make vitrified powder mixed with kneaded polyolefin, silicone rubber, silicon dioxide, silicone oil, platinum complex and / or platinum compound, coupling agent, antioxidant The agent and flame retardant are mixed evenly to form a group of ceramic rubber;
[0078] ④ move the lumpy ceramic rubber out of the kneade...
Embodiment 1
[0102]Get 100 parts of polyethylene, 20 parts of silicon dioxide, 1 part of methyl silicone oil, 0.01 part of 1000ppm isopropanol solution of chloroplatinic acid, 0.1 part of KH560 coupling agent, 20 parts of red phosphorus, and 20 parts of aluminum oxide, According to the first preparation method of the above-mentioned flame-retardant ceramic composite material, the flame-retardant ceramic composite material is prepared. When the flame-retardant ceramic composite material is vulcanized and formed, 1 part of 2,5-dimethyl-2,5-bis (tert-butylperoxy)hexane.
Embodiment 2
[0104] Take 100 parts of ethylene-vinyl acetate copolymer (EVA), 100 parts of silicon dioxide, 30 parts of hydroxyl silicone oil, 10 parts of 1000ppm isopropanol solution of chloroplatinic acid, 0.1 part of A171 coupling agent, 100 parts of red phosphorus, 150 parts of silicon dioxide, according to the first preparation method of the above-mentioned flame-retardant ceramic composite material, the flame-retardant ceramic composite material is prepared. When the flame-retardant ceramic composite material is vulcanized and formed, 2 parts of 2,4-dichloroperoxide Benzoyl oxide (commonly known as double ~ two four).
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