Novel method for post-processing vat yellow GCN
A new method and crude technology, applied in the field of dyes, can solve problems such as inability to completely control
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0020] Add 17.5 grams of vat yellow GCN crude product (intensity compared with the standard is 90.27%; brightness difference (DC) is 3.38) into 175 grams of tetrachloroethylene, stir and heat to 120 ° C, reflux for 6 hours, cool to room temperature and filter. The filter cake was washed three times with 33 grams of tetrachlorethylene, and sucked dry. Add 99 grams of water to the above-mentioned naphthalene-free filter cake for beating, add 34 grams of 30% hydrochloric acid and 0.45 grams of sodium chlorate, slowly heat to 80 ° C under stirring, and keep warm for 2 hours. Filter while it is hot, wash the filter cake until neutral drying, and obtain 10 grams of pretreated reduced yellow GCN dry product. Add 185 grams of concentrated sulfuric acid solution with a concentration of 50% by weight to the above-mentioned dry product, stir and heat up to 150°C for 2 hours, then take a sample, observe with a microscope, if the crystal becomes transparent, the end point of the crystal tr...
Embodiment 2
[0021] Take 10 grams of the above pretreated vat yellow GCN dry product, add 205 grams of sulfuric acid concentrated solution with a concentration of 50% by weight, stir and heat up to 140 ° C for 3 hours, then take a sample, observe with a microscope, if the crystal becomes transparent, it means the end point of crystal transformation To, down to room temperature, add 77 grams of water to isolate the material, the material is suction filtered, and the mother liquor is collected. Subsequent operations were the same as above to obtain 9.8 grams of reduced yellow GCN dry product. Compared with the standard, the intensity is 216.87%, and the brightness difference (DC) is 0.61.
Embodiment 3
[0023] Take 10 grams of the above-mentioned pretreated vat yellow GCN dry product, add 225 grams of sulfuric acid concentrated solution with a concentration of 50% by weight, stir and heat up to 130 ° C for 4 hours, then take a sample, observe with a microscope, if the crystal becomes transparent, it means the end point of crystal transformation To, down to room temperature, add 57 grams of water to isolate the material, the material is suction filtered, and the mother liquor is collected. Subsequent operations were the same as above to obtain 9.5 grams of reduced yellow GCN dry product. Compared with the standard, the strength is 204.85%, and the brightness difference (DC) is 0.68.
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com