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Preparation method of xylitol and maltitol eutectic

A technology of maltitol and crystallized maltitol, which is applied in the field of preparation of xylitol and maltitol co-crystals, can solve problems such as difficult large-scale production, difficulty in crushing, and large power consumption, and achieve good economic benefits and social significance. Machinability, effect of expanding application range

Active Publication Date: 2014-01-15
山东绿健生物技术有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Patent ZL200680003064.0 mentions the preparation method of xylitol and maltitol co-crystals. This method prepares co-crystals. Due to the low kneading temperature, the molten sugar alcohol is already in a very viscous state at this temperature. Add seed crystals Post-kneading is difficult and takes a long time, so the power consumption is large, and the aging time is long, and it is difficult to crush, so it is not easy to achieve large-scale production
The preparation method of the xylitol co-crystal introduced in the patent ZL200910310390.1 uses too few crystal seeds, so the crystallization speed is very slow, and at the same time, the crystal seeds are easy to dissolve, so the production efficiency is low; The easy hygroscopicity of xylitol, the deficiencies that are difficult to compress make it more suitable for preparing gummies and tabletting, expanding the application range of xylitol, but because this kind of co-crystal is the co-crystal of xylitol and sorbitol , the astringency of monosaccharide alcohols has not been improved, so there are deficiencies in the application

Method used

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  • Preparation method of xylitol and maltitol eutectic
  • Preparation method of xylitol and maltitol eutectic

Examples

Experimental program
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Effect test

Embodiment 1

[0020] Embodiment 1 prepares xylitol and maltitol co-crystal

[0021] Mix crystalline xylitol and crystalline maltitol at a mass ratio of 10:1, then heat to a molten state with a solid mass fraction of 99.5%, drop the temperature to 120°C and add it to the seed crystal, which is crystalline xylitol and A mixture of crystallized maltitol, the ratio of xylitol and maltitol in the mixture is the same as that in the molten state, the amount of seed crystals used is 1 / 2 of the mass of the molten state, stirring while adding, so that the two are mixed evenly, and then passed The temperature is 25°C, the humidity is 35% of dry cold air for drying and cooling, the cooling rate is 15°C / h, and after cooling to 40°C, it is pulverized to obtain xylitol and maltitol co-crystals, which are displayed in differential scanning calorimetry. A single melting peak (eg figure 1 shown).

Embodiment 2

[0022] Embodiment 2 prepares xylitol and maltitol co-crystal

[0023] Mix crystalline xylitol and crystalline maltitol at a mass ratio of 2:1, then heat to a molten state with a solid mass fraction of 99.0%, drop the temperature to 160°C and add it to the seed crystal, which is crystalline xylitol and A mixture of crystalline maltitol. The ratio of xylitol and maltitol in the mixture is the same as that in the molten state. The amount of seed crystals used is twice the mass of the molten state. Stir while adding to make the two mix evenly, and then pass into the temperature 20°C, dry cold air with a humidity of 30% for dry cooling, the cooling rate is 5°C / h, cooled to 30°C and then pulverized to obtain xylitol and maltitol co-crystals.

Embodiment 3

[0024] Embodiment 3 prepares xylitol and maltitol co-crystal

[0025] Mix crystalline xylitol and crystalline maltitol at a mass ratio of 5:1, then heat to a molten state with a solid mass fraction of 99.2%, cool down to 150°C and add to the seed crystals, which are xylitol and maltose Alcohol co-crystal, the proportion of xylitol and maltitol in the co-crystal is the same as that in the molten state, the amount of seed crystal used is the same as that in the molten state, stir while adding, so that the two are evenly mixed, and then the temperature of feeding is 22°C , the dry cold air with a humidity of 32% was dried and cooled at a cooling rate of 10°C / h, cooled to 35°C and crushed to obtain xylitol and maltitol co-crystals.

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Abstract

The invention discloses a preparation method of xylitol and maltitol eutectic, which comprises the following steps that raw xylitol and raw maltitol are mixed at a mass ratio of (10:1)-(2:1), and evaporated and concentrated to a molten state that the mass fraction of solid in a mixture is above 98%; a molten-state xylitol and maltitol mixture is obtained, cooled to 120-160 DEG C, mixed with a seed crystal, and stirred sufficiently, so that the molten-state xylitol and maltitol mixture is eutectic; cooling and drying are performed after uniform mixing; the temperature is reduced to 30-40 DEG C; smashing is performed; and the xylitol and maltitol eutectic is obtained. The method solves the problems that the kneading difficulty is great, the ageing time is long, the smashing is difficult, the crystallization speed is low, the efficiency is low, and mass production is not easy in the existing production technology of the eutectic. The xylitol and maltitol eutectic prepared by the method has good homogeneity, is more suitable for preparing chewing gum and preforming, and has good economic benefits and social significance.

Description

technical field [0001] The invention relates to a preparation method of xylitol and maltitol co-crystal, belonging to the field of biotechnology. Background technique [0002] Both xylitol and maltitol are functional sweeteners, which are not easy to cause dental caries after eating, and will not increase blood sugar, so they are widely used as sweeteners in the food industry. In addition to the above common points, the two sugar alcohols also have their own characteristics. Sometimes it is necessary to mix the two sugar alcohols, but due to the different size, shape, particle size and specific gravity of the powder particles, segregation often occurs, which has great impact on food processing and The quality is very negative. Therefore, it is imperative to prepare a composition of xylitol and maltitol with excellent processability such as uniformity. [0003] Patent ZL200680003064.0 mentions the preparation method of xylitol and maltitol co-crystals. This method prepares ...

Claims

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Application Information

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IPC IPC(8): A23L1/236A23L27/30
CPCA23L27/34A23L29/37A23V2002/00A23V2200/08A23V2250/6422A23V2250/6416
Inventor 信成夫景文利于丽任尚美刘建范静陈永芹
Owner 山东绿健生物技术有限公司
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