High-temperature resistant oil well rubber sealing ring material and preparation method thereof

A technology of rubber sealing ring and high temperature resistance, applied in the field of rubber materials, can solve the problems of reduced service life, aging and loss of rubber sealing packing, etc., and achieve poor compatibility and adhesion, good high temperature resistance, and reduced raw material costs Effect

Active Publication Date: 2014-01-08
CHANGZHOU UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The study found that in the process of crude oil extraction, the rod pumping equipment plays a major decisive role, and the wellhead polished rod sealing device is the most important in the rod pumping equipment, and the sealing device in the wellhead sealing device of the pumping unit The packing produces sliding friction with the sucker rod 24 hours a day, and the temperature difference across the country is very large, which will accelerate the aging of rubber sealing packing commonly used in oil fields, reduce its service life, and more seriously, cause Oil spill
At present, the sealing packing materials used in the market are mainly various kinds of packing, such as graphite packing, aramid packing, PTFE packing, carbon fiber packing, which have strong temperature resistance and solvent resistance. The research found that , the biggest problem facing the packing during use is frequent failure. The service life of oil wells with relatively harsh environments is less than 24 hours, and the best is only 1 to 2 months. If in the actual production process, the packing fails and there is no If it is discovered in time and appropriate remedial measures are taken, oil and gas will leak and cause environmental pollution and other problems, and more seriously, large-scale fires will occur, causing certain harm and loss to the country's energy and people's health

Method used

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  • High-temperature resistant oil well rubber sealing ring material and preparation method thereof
  • High-temperature resistant oil well rubber sealing ring material and preparation method thereof
  • High-temperature resistant oil well rubber sealing ring material and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0042] Inner glue:

[0043]

[0044] middle layer:

[0045]

[0046] Outer glue:

[0047]

[0048] (1) According to the formula in Example 1, except for the high-strength woven fabric, the raw materials of the inner and outer layer rubber and the middle layer are weighed, blended and mixed by an open mill or an internal mixer, and the mixed rubber powder is filtered separately To remove impurities to obtain pre-rubber powder;

[0049] (2) Put the pre-rubber powder obtained in step (1) through a cold-feed compound extruder (SH-36, Nanjing Jieya Extrusion Equipment Co., Ltd., the temperature of the extruder is set between 80-100°C) Extrude the inner, outer and middle layers of glue. When extruding, control the thickness of the glue layer to 10mm, and cut it into the specified size according to the need;

[0050] (3) In the order of "rubber-woven cloth-rubber-woven cloth-rubber", add the inner layer glue, middle layer glue, outer layer glue and woven cloth cut out in st...

Embodiment 2

[0054] Inner glue:

[0055]

[0056] middle layer:

[0057]

[0058] Outer glue:

[0059]

[0060] The preparation method of this embodiment is similar to that of Example 1. During the preparation process: the thickness of the extruded rubber layer is 8 mm, the thickness of the added woven cloth is 0.4 mm, and the inner and outer layers are set to have a 4-layer structure, and the middle layer is 5-layer structure, the vulcanization time is 25min, and the vulcanization temperature is 165°C.

Embodiment 3

[0062] Inner glue:

[0063]

[0064] middle layer:

[0065]

[0066] Outer glue:

[0067]

[0068] The preparation method of this embodiment is similar to that of Example 1. In the preparation process: the thickness of the extruded rubber layer is 4mm, the thickness of the added woven cloth is 0.1mm, and the inner and outer layers are set to be 7-layer structure, and the middle layer is 5-layer structure, vulcanization time is 20min, and vulcanization temperature is 150°C.

[0069] The performance test of the finished product prepared by above-mentioned 3 embodiments is as follows:

[0070]

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Abstract

The invention provides a high-temperature resistant oil well rubber sealing ring material and a preparation method thereof. The rubber sealing ring material is composed of three parts: the inner layer and the outer layer are both composed of high-strength knitted cloth added with inorganic materials such as carbon black, nano zirconia, and the like; the middle layer is prepared through following steps: compounding rubber powder, which has been desulfurated through thermal mechanical shearing, with fluoro-rubber, adding a compatilizer to increase the compatibility between the rubber powder and the fluoro-rubber; then adopting high-strength knitted cloth, which has been subjected to a surface treatment, as the support body, adding inorganic filling materials such as carbon black, nano zirconia, and the like, and subjecting the knitted cloth added with inorganic filling materials to a high-temperature sulfide cross-linked forming so as to obtain the middle layer. The sealing ring knitted cloth and the rubber base material are subjected to processes of multi-layer compounding and sulfide forming. The sealing ring prepared by the invention has a good high-temperature resistant performance, and is capable of being used in areas with a large temperature difference for a long period.

Description

technical field [0001] The invention belongs to the technical field of rubber materials, in particular to a rubber sealing ring material and a preparation method thereof. Background technique [0002] Petroleum is a basic energy closely related to people's lives. The rapid development of the petroleum industry plays a very important role in the development of the national economy. As the amount of recoverable crude oil decreases year by year, the importance of achieving sustainable development, crude oil extraction The efficiency of oil production and the improvement of ultimate recovery factor have gradually become the issues considered by oil workers. [0003] The study found that in the process of crude oil extraction, the rod pumping equipment plays a major decisive role, and the wellhead polished rod sealing device is the most important in the rod pumping equipment, and the sealing device in the wellhead sealing device of the pumping unit The packing produces sliding f...

Claims

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Application Information

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IPC IPC(8): B32B25/10B32B17/06B32B37/02C08L27/12C08L29/10C08L17/00C08L23/26C08K3/04C08K3/22F16J15/20
Inventor 陶国良夏艳平
Owner CHANGZHOU UNIV
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