PET composite material and preparation method thereof
A technology of composite materials and compounds, which is applied in the field of low-temperature-resistant halogen-free flame-retardant PET composite materials and its preparation, can solve the problems of low-temperature resistance and flame-retardant performance of PET materials, and achieve the effects of low cost, simple process, and elimination of influence
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[0036] The embodiment of the present invention further provides the above PET composite material preparation method, comprising the following steps:
[0037] Step S01, providing raw materials:
[0038] Weigh the thermoplastic polyester elastomer, PET, halogen-free flame retardant, compatibilizer, coupling agent and dispersant according to the formula;
[0039] Step S02, preparing the first mixture:
[0040] mixing the halogen-free flame retardant and coupling agent in a high mixer for 10 to 20 minutes to obtain the first mixture;
[0041] Step S03, preparing the second mixture:
[0042] mixing the first mixture, PET, dispersant, and dried thermoplastic polyester elastomer and compatibilizer to obtain a second mixture;
[0043] Step S04, extrusion process:
[0044] The second mixture is melt-extruded to obtain a PET composite material.
[0045] Specifically, in step S01, the thermoplastic polyester elastomer, PET, halogen-free flame retardant, compatibilizer, coupling agen...
Embodiment 1
[0052] Embodiment PET composite material of the present invention, comprises the component of following parts by weight:
[0053] 5 parts of TPEE 7246; 82 parts of PET 1100; 3 parts of 790; 0.1 part of KH560; 0.1 part of ADR-4370; 9 parts of OP1240; 1 part of MR01;
Embodiment PE
[0054] The preparation method of the PET composite material of the embodiment of the present invention comprises the following steps:
[0055] a: Weigh the components with the above contents, first dry the thermoplastic polyester elastomer and compatibilizer in a vacuum oven at 45°C for 3-4 hours;
[0056] b: uniformly mixing the halogen-free flame retardant and the coupling agent in a high-speed mixer to obtain the first mixture;
[0057] c: Add the PET resin, dispersant, thermoplastic polyester elastomer and compatibilizer dried in step a to the first mixture, and continue mixing until uniform to obtain a second mixture;
[0058] d: Put the second mixture mixed in step c into the hopper of the twin-screw extruder, melt and extrude, and granulate; The temperature in the zone is 190°C, the temperature in the fourth zone is 200°C, the head is 220°C, the speed of the main engine is 450 rpm, and the pressure is 18MPa.
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