Nano composite core material of energy accumulating vacuum insulated panel and preparation method thereof
A technology of nano-composite core material and vacuum insulation board, which is applied in the field of nano-composite core material and preparation, can solve the problems of inability to obtain thermal conductivity at room temperature, low heat insulation material, difficult heat insulation requirements, etc., and achieves excellent heat insulation effect, room temperature Low thermal conductivity and reduced complexity
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Embodiment 1
[0024] The concrete steps of preparation are:
[0025] In step 1, the modifying agent, ethanol and water are first mixed according to the weight ratio of 0.1:100:1; wherein, the modifying agent is ethyltriethoxysilane to obtain a modifying liquid. The modifying liquid is atomized by an atomizer, sprayed onto the nanoparticles and stirred evenly; wherein, the weight ratio of the modifying agent in the modifying liquid to the nanoparticles is 0.001:1, and the nanoparticles are silicon oxide. Next, bake the nanoparticles coated with the modifying agent at 55° C. for 10 hours to obtain nanometer powder.
[0026] Step 2, first place the nanopowder, phase change energy storage microcapsules, radiation barrier and organic fiber in a closed mixer with a weight ratio of 100:10:10:8, and place them at a speed of 100r / min Mix for 60 minutes; wherein, the radiation blocking agent is silicon carbide, and the organic fiber is polyester fiber to obtain a mixture. Spraying concentration is ...
Embodiment 2
[0029] The concrete steps of preparation are:
[0030] In step 1, the modifying agent, ethanol and water are first mixed according to the weight ratio of 0.5:100:3; wherein, the modifying agent is ethyltriethoxysilane to obtain a modifying liquid. Then, the modifying liquid is atomized by an atomizer, sprayed onto the nanoparticles and stirred evenly; wherein, the weight ratio of the modifying agent in the modifying liquid to the nanoparticles is 0.003:1, and the nanoparticles are silicon oxide. Next, the nanoparticles coated with the modifier on the surface were baked at 58° C. for 9 hours to obtain nanopowders.
[0031] Step 2, first place the nanopowder, phase change energy storage microcapsules, radiation barrier and organic fiber in a closed mixer with a weight ratio of 100:19:5:11, and place them at a speed of 1000r / min Mix for 45 minutes; wherein, the radiation blocking agent is silicon carbide, and the organic fiber is polyester fiber to obtain a mixture. Spraying co...
Embodiment 3
[0034] The concrete steps of preparation are:
[0035] In step 1, the modifying agent, ethanol and water are first mixed according to the weight ratio of 1:100:5; wherein, the modifying agent is ethyltriethoxysilane to obtain a modifying liquid. The modifying solution is atomized by an atomizer, sprayed onto the nanoparticles and stirred evenly; wherein, the weight ratio of the modifying agent in the modifying solution to the nanoparticles is 0.005:1, and the nanoparticles are silicon oxide. Next, bake the nanoparticles coated with the modifying agent at 60° C. for 8 hours to obtain nanometer powder.
[0036] Step 2, first place the nanopowder, phase change energy storage microcapsules, radiation barrier and organic fiber in a closed mixer with a weight ratio of 100:28:1:14, and place them at a speed of 2500r / min Mix for 30 minutes; wherein, the radiation blocking agent is silicon carbide, and the organic fiber is polyester fiber to obtain a mixture. Spray the adhesive that ...
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