Adhesive for solid wood floor and preparation method thereof
A technology of solid wood flooring and adhesives, applied in the direction of adhesives, adhesive additives, adhesive types, etc., can solve the problems of unusable stability and bad noise of solid wood floors, and achieve good elasticity and strong adhesion , Improve thixotropic performance, improve the effect of elasticity
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[0037] The preparation method of the solid wood floor adhesive of the embodiment of the present invention comprises:
[0038] Get the raw materials of the adhesive according to the above formula;
[0039] (1) Dehydration of polyether polyol: Add polyether polyol into the reaction kettle, stir and heat up to 110-120°C, vacuumize and dehydrate for 2 hours;
[0040] (2) Preparation of prepolymer: Add polyisocyanate to the dehydrated polyether polyol, stir and heat to 70-80°C, keep warm for 3-4h to prepare prepolymer
[0041] (3) Filler dehydration: put the filler in a drying room at 105-120°C, and bake the material for 3-5h;
[0042](4) Preparation of environmentally friendly elastic paving adhesive for solid wood flooring:
[0043] Add the plasticizer, the prepolymer prepared in step (2), and the dewatering agent into the planetary stirring tank, evacuate until the vacuum degree is 0.095MPa~-0.1MPa and stir for 1h; the dehydrated filler, antioxidant Add it into the planetary ...
Embodiment 1
[0051] This embodiment provides an adhesive that can realize elastic paving of solid wood floors, improve the stability of solid wood floors after paving, reduce noise, and can be used in floor heating systems. The adhesive is prepared by the following steps (wherein Each component is weight part):
[0052] (1) Dehydration of polyether polyols: Add 24.5 parts of polyoxypropylene triol with an average molecular weight of 7300, 3.5 parts of castor oil, and 7 parts of polytetrahydrofuran diol with an average molecular weight of 2000 into the reactor, stir and heat to 115 ℃, vacuum dehydration for 2 hours, and cool down;
[0053] (2) Preparation of prepolymer: Add 3.5 parts of PAPI, 0.7 parts of NDI, and 2.8 parts of MDI to the dehydrated polyoxypropylene triol, castor oil and polytetrahydrofuran diol, stir and heat to 75 ° C, keep warm for 3 hours, and form Prepolymer;
[0054] (3) Filler dehydration: put 20 parts of nano-calcium carbonate, 18 parts of nano-talc powder, 12 part...
Embodiment 2
[0058] This embodiment provides an adhesive that can realize the elastic paving of solid wood floors, improve the stability of solid wood floors after paving, prevent hollowing, reduce noise, and can be used in floor heating systems. The agent is prepared through the following steps (wherein each component is parts by weight):
[0059] (1) Dehydration of polyether polyols: Add 18 parts of polyoxypropylene triols with an average molecular weight of 5000 and 2 parts of polyoxypropylene diols with an average molecular weight of 1000 into the reaction kettle, stir and heat up to 115°C, then vacuumize Dehydrate for 2 hours, cool down;
[0060] (2) Preparation of prepolymer: add 1 part of PAPI, 0.5 part of NDI, and 3.5 parts of TDI to the dehydrated polyoxypropylene triol and polyoxypropylene diol, stir and heat to 75 ° C, keep warm for 4 hours, and generate a prepolymer ;
[0061] (3) Filler dehydration: Put 10.38 parts of nano-calcium carbonate, 18 parts of nano-kaolin, 1.5 part...
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