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Preparation method of energy-storage light-emitting concrete

A technology of energy storage and luminescence, concrete, applied in the direction of luminescent materials, chemical instruments and methods, etc.

Inactive Publication Date: 2013-03-13
SHENYANG JIANZHU UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

But they all have shortcomings. Quartz polyurethane and protective film increase the cost, and the process operation is complicated, which is not conducive to on-site operation, and the properties of luminescent materials also affect the luminous properties and cost of concrete.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] (a) CaO:xDy 3+ , yNa + Preparation of phosphor powder: CaCO 3 , Na 2 CO 3 (both are analytically pure) and Dy 2 o 3 (99.99%, analytically pure) weighed accurately according to the molar ratio Ca:Dy:Na=l:0.01:0.1, added a small amount of ethanol (as a grinding aid), fully ground evenly, and dried in an oven at 110°C for 3 hours. The precursor was obtained, calcined at 950°C for 2 hours, cooled, and ground to obtain white powdery phosphor; (b) Preparation of luminous concrete: according to the mass percentage of each component, phosphor powder 4%, white cement 18%, standard sand 27%, stone 43%, water 8% and accurately weigh various substances; clean the weighed gravel and dry it, put the dried gravel, cement, standard sand, water and fluorescent powder together Stir in the blender, after stirring evenly, put the mixture into the mold, remove the mold after 24 hours, and then put the test block into the standard curing box for curing.

Embodiment 2

[0020] (a) CaO:xDy 3+ , yNa + Preparation of phosphor powder: CaCO 3 , Na 2 CO 3 (both are analytically pure) and Dy 2 o 3 (99.99%, analytically pure) according to the molar ratio Ca:Dy:Na=l:0.015:0.2, accurately weighed, added a small amount of ethanol (as a grinding aid), fully ground evenly, and dried in an oven at 110°C for 3 hours. The precursor was obtained, calcined at 1050°C for 2.5h, cooled, and ground to obtain white powdery phosphor; (b) Preparation of luminous concrete: according to the mass percentage of each component, phosphor powder 6%, white cement 18%, standard 27% of sand, 41% of stone, and 8% of water are used to accurately weigh various substances; clean and dry the weighed gravel, and put the dried gravel, cement, standard sand, water and fluorescent powder together Put it into a mixer for stirring, and after stirring evenly, put the mixture into a mold, remove the mold after 24 hours, and then put the test block into a standard curing box for curi...

Embodiment 3

[0022] (a) CaO:xDy 3+ , yNa + Preparation of phosphor powder: CaCO 3 , Na 2 CO 3 (both are analytically pure) and Dy 2 o 3 (99.99%, analytically pure) according to the molar ratio Ca:Dy:Na=l:0.02:0.2, accurately weighed, added a small amount of ethanol (as a grinding aid), fully ground evenly, and dried in an oven at 110°C for 3 hours. The precursor was obtained, calcined at 1150°C for 3 hours, cooled, and ground to obtain white powder phosphor; (b) Preparation of luminous concrete: according to the mass percentage of each component, phosphor powder 8%, white cement 18%, standard sand 27% %, stone 39%, water 8% and accurately weigh various substances; clean the weighed gravel and dry it, put the dried gravel, cement, standard sand, water and fluorescent powder into the mixer together Stir in the medium, stir the mixture evenly, put the mixture into the mold, remove the mold after 24 hours, and then put the test block into the standard curing box for curing.

[0023] In...

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PUM

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Abstract

The invention relates to light-emitting concrete, particularly a preparation method of energy-storage light-emitting concrete. The energy-storage light-emitting concrete is prepared from the following raw materials in percentage by weight: 2-8% of fluorescent powder, 18% of white cement, 27% of standard sand, 39-47% of gravel and 8% of water. The CaO:Dy3+,Na+ fluorescent powder is prepared from initial raw materials CaCO3 (analytically pure), Na2CO3 (analytically pure) and Dy2O3 (99.99%, analytically pure) in a Ca:Dy:Na mol ratio of l:x:y, and a small amount of ethanol is added as a grinding aid. The prepared CaO:Dy3+,Na+ fluorescent powder has the advantages of no pollution, no radiation, favorable light-emitting performance and simple production technique, and has the meanings in environmental protection and energy saving. The prepared light-emitting concrete has the advantages of long light-emitting time and no radioactivity; and after being irradiated under sunlight in the day time or under a common daylight lamp for 50 minutes, the light-emitting concrete can continuously emit light in a dark place for more than 6 hours.

Description

technical field [0001] The invention relates to a luminescent concrete, in particular to a luminescent concrete which absorbs sunlight or ultraviolet light during the day, stores light energy, and releases the stored light energy in the form of visible light at night and a preparation method thereof. Background technique [0002] Long afterglow luminescent material is a new type of functional material that absorbs sunlight or ultraviolet light during the day, stores the light energy, and releases the stored light energy in the form of visible light at night when the light stops shining. Long afterglow materials themselves cannot be directly used as end products, and must be combined with other materials to be applied. Concrete is the most commonly used material in the construction industry, and it is widely used in the construction of some public facilities. Therefore, the development and innovation research of concrete is quite important. important and has a bright future. ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B28/04C09K11/55
Inventor 赵苏王倩田中心富尔康
Owner SHENYANG JIANZHU UNIVERSITY
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