Super-nylon 66 alloy prepared by in-situ reactive compatibilization method and preparation method thereof

A nylon and super-tough technology, applied in the field of nylon 66 alloy, can solve the problems of poor mechanical properties of the blend, and achieve the effects of easy popularization and application, easy control, and improved production efficiency

Inactive Publication Date: 2012-11-28
SINOPLAST NEW MATERIAL
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, POE is a non-polar elastomer, and the mechanical properties of the blend obta...

Method used

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  • Super-nylon 66 alloy prepared by in-situ reactive compatibilization method and preparation method thereof
  • Super-nylon 66 alloy prepared by in-situ reactive compatibilization method and preparation method thereof
  • Super-nylon 66 alloy prepared by in-situ reactive compatibilization method and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0050] Super-tough nylon 66 alloy prepared by in-situ reaction compatibilization method is composed of the following raw materials in parts by weight: 90 parts of polyamide 66 (PA66), 10 parts of ethylene and octene copolymer (POE), 2,5-dimethyl - 0.1 part of 2,5-di-tert-butylperoxyhexane (L-101), 0.5 part of maleic anhydride (MAH).

[0051] The method for preparing super-tough nylon 66 alloy by in-situ reaction compatibilization method comprises the following steps:

[0052] (1), the initiator 2,5-dimethyl-2,5-di-tert-butylperoxyhexane and maleic anhydride are dissolved in acetone, and placed for later use;

[0053] (2) Put nylon 66 in a vacuum oven for drying treatment, control the oven temperature at 90°C, dry for 4 hours, place POE in a vacuum oven for drying treatment, control the oven temperature at 70°C, and dry for 4 hours, Nylon 66 and POE were then cooled to room temperature;

[0054] (3), pour the mixed solution of initiator 2,5-dimethyl-2,5-di-tert-butylperoxyhex...

Embodiment 2

[0057] Super-tough nylon 66 alloy prepared by in-situ reaction compatibilization method is composed of the following raw materials in parts by weight: 80 parts of polyamide 66 (PA66), 20 parts of ethylene and octene copolymer (POE), 2,5-dimethyl - 0.5 parts of 2,5-di-tert-butylperoxyhexane (L-101), 2.5 parts of maleic anhydride (MAH).

[0058] The method for preparing super-tough nylon 66 alloy by in-situ reaction compatibilization method, its steps are the same as in Example 1.

Embodiment 3

[0060] Super-tough nylon 66 alloy prepared by in-situ reaction compatibilization method is composed of the following raw materials in parts by weight: 70 parts of polyamide 66 (PA66), 30 parts of ethylene and octene copolymer (POE), 2,5-dimethyl - 0.1 part of 2,5-di-tert-butylperoxyhexane (L-101), 1 part of maleic anhydride (MAH).

[0061] The method for preparing super-tough nylon 66 alloy by in-situ reaction compatibilization method, its steps are the same as in Example 1.

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Abstract

The invention discloses super-nylon 66 alloy prepared by an in-situ reactive compatibilization method and a preparation method thereof, and the preparation method is used for improving the compatibility of nylon 66 and POE (poly ortho ester), and preparing the super-nylon 66 alloy with high toughness, low temperature resistance and low water absorption rate. The super-nylon 66 alloy comprises the following compounds in parts by weight: 55 to 95 parts of nylon 66, 5 to 45 parts of POE, 0.01 to 1 part of initiating agent, and 0.1 to 4 parts of maleic anhydride, wherein the initiating agent is organic peroxide. The super-nylon 66 alloy provided by the invention has excellent comprehensive performance, in particular high notch impact strength, excellent low temperature impact resistance and low water absorption rate; and the product can be used in producing various automobile parts, mechanical parts, electronic appliances, package materials and the like with high toughness, abrasion resistance and excellent self-lubrication performance.

Description

technical field [0001] The invention belongs to the field of materials, and in particular relates to a method for preparing a nylon 66 alloy with high toughness, low temperature resistance and low water absorption by using an in-situ reaction compatibilization method. Background technique [0002] Polyamide, also known as nylon (PA), is the basic resin with the widest application, the largest variety, the largest output, and excellent comprehensive performance among the five general-purpose engineering plastics. PA66 is a translucent or opaque milky white crystalline polymer. It has the advantages of high strength, wear resistance, solvent resistance and wide temperature range. It is widely used in automobile manufacturing, mechanical equipment, electronic appliances, medical equipment and precision instruments. However, due to the characteristics of strong polarity, PA66 has the disadvantages of strong hygroscopicity, poor dimensional stability, and low notched impact stren...

Claims

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Application Information

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IPC IPC(8): C08F283/04C08F255/02C08F4/28C08J3/24B29B9/06B29B13/06
Inventor 朱怀才王忠强
Owner SINOPLAST NEW MATERIAL
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