Applications of tea polyphenol/beta-cyclodextrin inclusion compound taken as cigarette filter additive in reduction of cigarette smoke phenolic compound
A technology of cyclodextrin inclusion compound and phenolic compound, which is applied in the fields of e-liquid filter element, tobacco, application, etc., can solve the problems of unfavorable cigarette smoke quality, smoke astringency and increased miscellaneous gas, etc., to achieve Good promotion and application value, convenient and easy operation, and simple adding method
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Embodiment 1
[0041] Weigh 360mg of β-cyclodextrin, add 5mL of distilled water, and heat to 60°C to dissolve it. Then weigh 180 mg of tea polyphenols and dissolve in 5 mL of absolute ethanol solution, and add dropwise into the aqueous solution of β-cyclodextrin under continuous stirring. Mixture through N 2 Protected, sealed and protected from light, and stirred at 60°C for 5h. Cool the mixture to room temperature, put it in the refrigerator for 24 hours, then filter it with suction, wash it quickly with distilled water and absolute ethanol, dry it in vacuum at 40°C for 6 hours, and grind it to obtain white tea polyphenol / β-cyclodextrin inclusion compound . Quantitatively weighed, added to the filter tip at a level of 7 mg / cigarette to make test cigarettes, and compared with control cigarettes. Except that the control cigarettes do not contain additives, other cigarette materials such as auxiliary materials, sizes, filter rods, etc. are exactly the same as the test cigarettes. The filte...
Embodiment 2
[0045] Weigh 400mg of β-cyclodextrin, add 8mL of distilled water, and heat to 50°C to dissolve it. Then weigh 200 mg of tea polyphenols and dissolve in 8 mL of absolute ethanol solution, and add dropwise into the β-cyclodextrin aqueous solution under constant stirring. Mixture through N 2 Protected, sealed and protected from light, and stirred at 50°C for 5h. Cool the mixture to room temperature, put it in the refrigerator for 24 hours, then filter it with suction, wash it quickly with distilled water and absolute ethanol, dry it in vacuum at 40°C for 6 hours, and grind it to obtain white tea polyphenol / β-cyclodextrin inclusion compound . Quantitatively weighed, added to the filter tip at the level of 10mg / cigarette to make test cigarettes, and compared with control cigarettes. Except that the control cigarettes do not contain additives, other cigarette materials such as auxiliary materials, sizes, filter rods, etc. are exactly the same as the test cigarettes. The filter s...
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