Method for rapidly tracing to water pollution source
A water pollution and fast technology, applied in the direction of material excitation analysis, fluorescence/phosphorescence, instruments, etc., can solve the problems of large cost investment, heavy maintenance workload, time-consuming and labor-consuming, etc., to strengthen supervision, strengthen supervision of sewage discharge, The effect of saving backtracking time
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Embodiment 1
[0047] After investigation, a representative manufacturer A of food production in the upper reaches of the North Canal in Huo County, Tongzhou, produces soybean paste, soy sauce, vinegar and other condiments. Collect the production sewage and waste water of manufacturer A, fill the sampling bottle with water samples without leaving space and air bubbles, affix a label and seal the mouth of the sampling bottle with sealing tape. The water samples were transported back to the laboratory on the same day and stored in a refrigerator at 4°C. The analysis and screening of anion species, organic species, metal elements and fluorescence information are carried out as follows:
[0048] Analysis and screening of anion type information: Take 20ml of water sample for vacuum filtration, dilute the filtrate 10 times with ultrapure water, and pass it through a 0.22μm microfiltration membrane for ion chromatography analysis. The conditions of ion chromatography are as follows: Dianne ICS-9000...
Embodiment 2
[0059] After investigation, the representative manufacturer B in the upper reaches of the North Canal in Huo County, Tongzhou, produces cooked duck food, hot pot bottom material, etc. Collect the production wastewater of manufacturer B, fill the sampling bottle with water sample without leaving space and air bubbles, label it and seal the mouth of the sampling bottle with sealing tape. The water samples were transported back to the laboratory on the same day and stored in a refrigerator at 4°C. The fingerprint information of the water sample is detected, extracted, analyzed and sorted, and the process and method are the same as in Example 1.
[0060] The sewage fingerprint obtained from manufacturer B is: anions include fluoride ion and phosphate ion; organic matter contains m-cresol, natural capsaicin, 2,4-di-tert-butylphenol, skatole, erucamide, oleic acid amide; characteristic metal The elements are Ti and Cr, and the corresponding concentrations are 4.31ppm and 0.15ppm; t...
Embodiment 3
[0065] After investigation, the representative manufacturer C of the chemical industry in the upper reaches of the North Canal in Huo County, Tongzhou, the product is polyacrylamide. Collect the production sewage and waste water of manufacturer C, fill the sampling bottle with water samples without leaving space and air bubbles, label and seal the mouth of the sampling bottle with sealing tape. The water samples were transported back to the laboratory on the same day and stored in a refrigerator at 4°C. The fingerprint information of the water sample is detected, extracted, analyzed and sorted, and the process and method are the same as in Example 1.
[0066] The sewage fingerprint obtained from manufacturer C is as follows: anions include fluoride, chlorite, chlorate, and bromate; organic matter acrylamide, 4-methoxyphenol, erucamide, oleamide, and methyl hexadecanoate; The metal elements are Cr and Ag, and the corresponding concentrations are 0.10ppm and 0.07ppm; the fluore...
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