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Preparation method and application of anti-blocking agent

An anti-caking agent and co-solvent technology, which is applied in the separation/purification of carboxylic acid compounds, organic chemistry, etc., can solve the problems of unsatisfactory anti-caking effect and no anti-caking agent, so that it is not easy to agglomerate, The effect of preventing grain agglomeration and preventing potassium formate from agglomerating

Inactive Publication Date: 2012-09-12
四川鸿康科技股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The above-mentioned anti-caking agent is mainly suitable for inorganic salt crystallization, and the anti-caking effect for organic salt crystallization such as potassium formate is not ideal
At present, there is no special anti-caking agent for potassium formate

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0041] The components (mass ratio) of the anti-caking agent 1 of the present embodiment are as follows:

[0042] Polyethylene glycol (400) 3.0kg (15 parts),

[0043] Lauryl alcohol polyoxyethylene (3) ether phosphate monoester 6.0kg (30 parts),

[0044] 2.0kg (10 parts) of acrylic acid-maleic anhydride polymer with a solid content of 30-100%,

[0045] Sodium methylene dinaphthalene sulfonate 5.0kg (25 parts),

[0046] Water 4.0kg (20 parts),

[0047] Preparation of anti-caking agent: Add polyethylene glycol (400) and lauryl polyoxyethylene (3) ether phosphoric acid monoester into the reaction kettle, stir and raise the temperature to 50°C, add acrylic acid-maleic anhydride polymer while keeping warm, and make Mix well, continue to stir and heat up to 60°C, add sodium methylene dinaphthalene sulfonate and water, continue to stir for 40 minutes to form a uniform solution, cool down to 30°C and pack to obtain the product.

[0048] Mixing method: the anti-caking agent is direc...

Embodiment 2

[0050] The components (mass ratio) of the anti-caking agent 2 of the present embodiment are as follows:

[0051] Polyethylene glycol (400) 1.0 kg (5 parts),

[0052] Lauryl alcohol polyoxyethylene (3) ether phosphate monoester 4.0 kg (20 parts),

[0053] 10.0 kg (50 parts) of acrylic acid-maleic anhydride polymer with a solid content of 30-100%,

[0054] Sodium methylene dinaphthalene sulfonate 3.0kg (15 parts),

[0055] Water 2.0kg (10 parts),

[0056] Preparation of anti-caking agent: Add polyethylene glycol (400) and lauryl polyoxyethylene (3) ether phosphoric acid monoester into the reaction kettle, stir and raise the temperature to 55°C, add acrylic acid-maleic anhydride polymer while keeping warm, and make Mix well, continue to stir and heat up to 70°C, add sodium methylene dinaphthalene sulfonate and water, continue to stir for 50 minutes to form a uniform solution, cool down to 30°C and pack to obtain the product.

[0057] Mixing method: the anti-caking agent is di...

Embodiment 3

[0059] The components (mass ratio) of the anti-caking agent 3 of the present embodiment are as follows:

[0060] Polyethylene glycol (400) 4.0kg (20 parts),

[0061] Lauryl alcohol polyoxyethylene (3) ether phosphoric acid monoester 1.8kg (9 parts),

[0062] 10.0kg (50 parts) of acrylic acid-maleic anhydride polymer with a solid content of 30-100%,

[0063] Sodium methylene dinaphthalene sulfonate 2.2kg (11 parts),

[0064] Water 2.0kg (10 parts),

[0065] Preparation of anti-caking agent: Add polyethylene glycol (400) and lauryl polyoxyethylene (3) ether phosphoric acid monoester into the reaction kettle, stir and raise the temperature to 50°C, add acrylic acid-maleic anhydride polymer while keeping warm, and make Mix well, continue to stir and heat up to 70°C, add sodium methylene dinaphthalene sulfonate and water, continue to stir for 30 minutes to form a uniform solution, cool down to 30°C and pack to obtain the product.

[0066] Mixing method: Spray the anti-caking ag...

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PUM

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Abstract

The invention discloses an anti-blocking agent, which comprises, by mass ratio, 3 parts to 25 parts of polyethylene glycol (400), 5 parts to 30 parts of dodecanol polyoxyethylene (3) phosphomonoester, 5 parts to 55 parts of crylic acid- malefic anhydride with solid content of 30% to 100%, and 1 part to 35 parts of disodium methylene dinaphthalenesulfonate. The anti-blocking agent is good in performance and little in dosage. Under the normal condition, the anti-blocking agent is added to potassium formate, the potassium formate can keep loose for 3 to 6 months, and The anti-blocking agent can not cause negtive effects on the quality and usage of the potassium formate after addition.The invention also discloses a preparation method and a usage method of the anti-blocking agent.

Description

technical field [0001] The invention relates to an anti-caking agent, in particular to a potassium formate anti-caking agent. Background technique [0002] At present, the total global production capacity of potassium formate in 2010 is 377,000 tons, and the domestic production capacity has reached more than 100,000 tons. It is mainly used in oil drilling, oil field drilling fluid, well completion fluid, surface activity modification of carbon black, deicing agent, mining and other fields. Globally, the application proportion of potassium formate in various fields is 93% in the oil field industry, 2.5% in the deicing agent industry, 1.5% in the leather industry, 1.5% in the printing and dyeing industry, and 1.5% in other industries. The drilling fluid and completion fluid composed of potassium formate fluid has many excellent characteristics: the density can be adjusted at will to meet various actual needs; it has good high temperature stability and strong inhibition; it is...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07C53/06C07C51/50
Inventor 萧棋仲毛逢银唐云郑世华豆永强
Owner 四川鸿康科技股份有限公司
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