Preparation method and application of anti-blocking agent
An anti-caking agent and co-solvent technology, which is applied in the separation/purification of carboxylic acid compounds, organic chemistry, etc., can solve the problems of unsatisfactory anti-caking effect and no anti-caking agent, so that it is not easy to agglomerate, The effect of preventing grain agglomeration and preventing potassium formate from agglomerating
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Embodiment 1
[0041] The components (mass ratio) of the anti-caking agent 1 of the present embodiment are as follows:
[0042] Polyethylene glycol (400) 3.0kg (15 parts),
[0043] Lauryl alcohol polyoxyethylene (3) ether phosphate monoester 6.0kg (30 parts),
[0044] 2.0kg (10 parts) of acrylic acid-maleic anhydride polymer with a solid content of 30-100%,
[0045] Sodium methylene dinaphthalene sulfonate 5.0kg (25 parts),
[0046] Water 4.0kg (20 parts),
[0047] Preparation of anti-caking agent: Add polyethylene glycol (400) and lauryl polyoxyethylene (3) ether phosphoric acid monoester into the reaction kettle, stir and raise the temperature to 50°C, add acrylic acid-maleic anhydride polymer while keeping warm, and make Mix well, continue to stir and heat up to 60°C, add sodium methylene dinaphthalene sulfonate and water, continue to stir for 40 minutes to form a uniform solution, cool down to 30°C and pack to obtain the product.
[0048] Mixing method: the anti-caking agent is direc...
Embodiment 2
[0050] The components (mass ratio) of the anti-caking agent 2 of the present embodiment are as follows:
[0051] Polyethylene glycol (400) 1.0 kg (5 parts),
[0052] Lauryl alcohol polyoxyethylene (3) ether phosphate monoester 4.0 kg (20 parts),
[0053] 10.0 kg (50 parts) of acrylic acid-maleic anhydride polymer with a solid content of 30-100%,
[0054] Sodium methylene dinaphthalene sulfonate 3.0kg (15 parts),
[0055] Water 2.0kg (10 parts),
[0056] Preparation of anti-caking agent: Add polyethylene glycol (400) and lauryl polyoxyethylene (3) ether phosphoric acid monoester into the reaction kettle, stir and raise the temperature to 55°C, add acrylic acid-maleic anhydride polymer while keeping warm, and make Mix well, continue to stir and heat up to 70°C, add sodium methylene dinaphthalene sulfonate and water, continue to stir for 50 minutes to form a uniform solution, cool down to 30°C and pack to obtain the product.
[0057] Mixing method: the anti-caking agent is di...
Embodiment 3
[0059] The components (mass ratio) of the anti-caking agent 3 of the present embodiment are as follows:
[0060] Polyethylene glycol (400) 4.0kg (20 parts),
[0061] Lauryl alcohol polyoxyethylene (3) ether phosphoric acid monoester 1.8kg (9 parts),
[0062] 10.0kg (50 parts) of acrylic acid-maleic anhydride polymer with a solid content of 30-100%,
[0063] Sodium methylene dinaphthalene sulfonate 2.2kg (11 parts),
[0064] Water 2.0kg (10 parts),
[0065] Preparation of anti-caking agent: Add polyethylene glycol (400) and lauryl polyoxyethylene (3) ether phosphoric acid monoester into the reaction kettle, stir and raise the temperature to 50°C, add acrylic acid-maleic anhydride polymer while keeping warm, and make Mix well, continue to stir and heat up to 70°C, add sodium methylene dinaphthalene sulfonate and water, continue to stir for 30 minutes to form a uniform solution, cool down to 30°C and pack to obtain the product.
[0066] Mixing method: Spray the anti-caking ag...
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