Method for preparing organic titanium-plant vinegar potassium salt organic fertilizer through salting-out process
A technology for planting vinegar potassium salt and organic titanium, applied in the application, fertilization device, fertilizer mixture and other directions, can solve the problems of undiscovered, miscellaneous belt, etc., and achieve the effect of excellent stability
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Embodiment 1
[0063] (1) Preparation of metatitanic acid:
[0064] a. Add 1000ml of ice water at 0°C~5°C to a 1500ml beaker, and add 10ml of hydrochloric acid and 20ml of titanium tetrachloride dropwise under the stirring of an electric stirrer to generate a titanium tetrachloride hydrochloric acid solution. The sodium hydroxide solution neutralizes the titanium tetrachloride hydrochloric acid solution, the temperature of the solution is controlled at ≤5°C, and the pH value is 7.0~8.0, so that metatitanic acid is precipitated in cold water at ≤5°C;
[0065] B, the newly precipitated metatitanic acid is washed with distilled water to remove chloride ions;
[0066] c. After the metatitanic acid that has been washed to remove chloride ions is removed by a centrifuge to remove part of the adsorbed water, it can be used for acid-soluble chelation.
[0067] (2) Preparation of titanium citrate chelate:
[0068] a. Preparation of citric acid-metatitanic acid suspension mixture:
[0069] The ti...
Embodiment 2
[0082] (1) Preparation of metatitanic acid:
[0083] a. Add 1000ml of ice water at 0°C~5°C to a 1500ml beaker, and add 10ml of hydrochloric acid and 20ml of titanium tetrachloride dropwise under the stirring of an electric stirrer to generate a titanium tetrachloride hydrochloric acid solution. The sodium hydroxide solution neutralizes the titanium tetrachloride hydrochloric acid solution, the temperature of the solution is controlled at ≤5°C, and the pH value is 7.0~8.0, so that metatitanic acid is precipitated in cold water at ≤5°C;
[0084] B, the newly precipitated metatitanic acid is washed with distilled water to remove chloride ions;
[0085] c. After the metatitanic acid that has been washed to remove chloride ions is removed by a centrifuge to remove part of the adsorbed water, it can be used for acid-soluble chelation.
[0086] (2) Preparation of titanium citrate chelate:
[0087] a. Preparation of citric acid-metatitanic acid suspension mixture:
[0088] The ti...
Embodiment 3
[0101] (1) Preparation of metatitanic acid:
[0102] a. Add 1000ml of ice water at 0°C~5°C to a 1500ml beaker, and add 10ml of hydrochloric acid and 20ml of titanium tetrachloride dropwise under the stirring of an electric stirrer to generate a titanium tetrachloride hydrochloric acid solution. The sodium hydroxide solution neutralizes the titanium tetrachloride hydrochloric acid solution, the temperature of the solution is controlled at ≤5°C, and the pH value is 7.0~8.0, so that metatitanic acid is precipitated in cold water at ≤5°C;
[0103] B, the newly precipitated metatitanic acid is washed with distilled water to remove chloride ions;
[0104] c. After the metatitanic acid that has been washed to remove chloride ions is removed by a centrifuge to remove part of the adsorbed water, it can be used for acid-soluble chelation.
[0105] (2) Preparation of titanium citrate chelate:
[0106] a. Preparation of citric acid-metatitanic acid suspension mixture:
[0107] The ti...
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