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Sanwei sandalwood granule and quality control method of preparation thereof

A technology of sandalwood and granules, which is applied in the field of medicine, can solve problems such as poor quality controllability, simple control standards, and simple quality standards, and achieve the effects of quality control, product quality safety, and improved identification

Active Publication Date: 2012-06-20
JINHE TIBETAN MEDICINE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the outstanding problems at present are simple quality standards and poor quality controllability
At present, the quality control methods for sanwei sandalwood granules in production still follow the outdated standards, the control standards are simple, and the means are single
For example, under the original quality standard, there are only gallic acid content determination items in jujube and gallic acid TLC identification items, which cannot effectively control the quality of other main components.
Therefore, the quality control of sanwei sandalwood granule products is not accurate, and the quality standard needs to be improved

Method used

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  • Sanwei sandalwood granule and quality control method of preparation thereof
  • Sanwei sandalwood granule and quality control method of preparation thereof
  • Sanwei sandalwood granule and quality control method of preparation thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0102] Embodiment 1: the quality control method of Sanwei Sandalwood Granules

[0103] Identification:

[0104] a. Identification of sandalwood

[0105] Take 5g of sanwei sandalwood granules, grind them finely, add 30ml of petroleum ether with a boiling range of 30-60°C, ultrasonically treat for 15 minutes, filter, evaporate the filtrate to dryness, add 2ml of petroleum ether with a boiling range of 60-90°C to dissolve the residue, and use it as the test sample Solution; take another 2g of sandalwood reference medicinal material, add 30ml of petroleum ether with a boiling range of 30-60°C, ultrasonically treat for 15min, filter, evaporate the filtrate to dryness, add 2ml of petroleum ether with a boiling range of 60-90°C to dissolve the residue, and use it as the reference medicinal material solution ; According to the test of thin-layer chromatography (Appendix VI B of "Pharmacopoeia of the People's Republic of China" in 2010), draw 4 μL of each of the above solutions, and p...

Embodiment 2

[0117] Embodiment 2: the quality control method of Sanwei Sandalwood Dropping Pills

[0118] Identification:

[0119] a. Identification of sandalwood

[0120] Take 7g of Sanwei Sandalwood Dropping Pills, grind finely, add 50ml of petroleum ether with a boiling range of 30-60°C, ultrasonically treat for 25min, filter, evaporate the filtrate to dryness, add 2ml of petroleum ether with a boiling range of 60-90°C to dissolve the residue, and use it as a test product. product solution; take another 2 g of sandalwood reference medicinal material, add 50 ml of petroleum ether with a boiling range of 30 to 60 ° C, ultrasonically treat for 15 to 25 minutes, filter, evaporate the filtrate to dryness, and add 2 ml of petroleum ether with a boiling range of 60 to 90 ° C to dissolve the residue as Control medicinal material solution; test according to thin-layer chromatography (Appendix VI B of "Pharmacopoeia of the People's Republic of China" 2010 Edition), draw 2-15 μL of each of the ab...

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Abstract

The invention discloses a detection method of a sanwei sandalwood granule, belonging to the technical field of medicine. The quality control method disclosed by the invention has the advantages of correspondingly improving the quality standard of the current sanwei sandalwood granule, increasing the verification of sandalwood and nutmeg in the sanwei sandalwood granule on the basis of the original standard, optimizing the verification of fructus choerospondiatis, and increasing a content measurement item of dehydrodiisoeugenol in the nutmeg so as to further guarantee the security, uniformity, stability and controllability of the product quality.

Description

technical field [0001] The invention relates to a quality control method of a traditional Chinese medicine compound preparation, in particular to a quality control method of Sanwei sandalwood granule and its preparation, belonging to the technical field of medicine. Background technique [0002] Sanwei Sandalwood Granules originated from the "Four Medical Codes" written by the medical sage Yutuo Yuandan Gonpo in the eighth century AD, and it is also recorded in "Tibetan Medicine Golden Prescription Collection" and "Tibetan Medicine Formula Collection" (Tibetan Edition). The original Tibetan name is "Zandan Sentang", which means "three-flavored sandalwood soup powder". After the clinical application and improvement of Tibetan medicine in the past dynasties, it has become a current prescription. It has the effects of promoting qi and blood circulation, promoting heart temperature, nourishing the heart and calming the nerves, and has a significant effect on angina pectoris caus...

Claims

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Application Information

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IPC IPC(8): G01N30/90G01N30/88
Inventor 孙泰俊李怀平单玉刚郑亭亭任松鹏
Owner JINHE TIBETAN MEDICINE
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