Epoxy resin composite wave-absorbing material and preparation method thereof
A composite absorbing material and epoxy resin technology, applied in the field of electromagnetic absorbing materials, can solve the problems of narrow absorbing frequency band, low absorbing efficiency, etc. Effect
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Embodiment 1~19
[0032] Examples 1-19 The preparation method of the composite wave-absorbing material is as follows:
[0033] (1) Put epoxy resin E-51 into a three-necked flask, heat and stir in a constant temperature water bath at 60°C, and after the epoxy resin E-51 becomes thinner, add magnetic fillers, conductive fillers and semiconductor fillers into the three-necked flask, Stir in a water bath at 60°C for 10 minutes, and the speed of the mixer is 400 rpm;
[0034] Wherein, the magnetic filler is one or more of nickel ferrite, zinc ferrite, manganese ferrite, zinc-nickel ferrite or zinc-manganese ferrite, and the particle size of the magnetic filler is 3 to 7μm;
[0035] The conductive filler is one or both of carbon fiber or carbon nanotube; the length of carbon fiber is 0.5-6mm, and the outer diameter of carbon nanotube is 5-50nm;
[0036] The semiconductor filler is one or both of aluminum-doped zinc oxide (ZAO) or tin-doped indium oxide (ITO); the particle size of the semiconductor ...
Embodiment 20~27
[0039] Examples 20-27 The preparation method of the composite wave-absorbing material is as follows:
[0040] (1) Put epoxy resin E-51 into a three-necked flask, heat and stir in a constant temperature water bath at 60°C, and after the epoxy resin E-51 becomes thinner, add magnetic fillers and conductive fillers into a three-necked flask, and place in a water bath at 60°C Stir for 10 minutes at a lower speed, and the speed of the mixer is 400 rpm;
[0041] Wherein, the magnetic filler is one or more of nickel ferrite, zinc ferrite, manganese ferrite, zinc-nickel ferrite or zinc-manganese ferrite, and the particle size of the magnetic filler is 3 to 7μm;
[0042] The conductive filler is one or both of carbon fiber or carbon nanotube; the length of carbon fiber is 0.5-6mm, and the outer diameter of carbon nanotube is 5-50nm;
[0043] (2) Put the curing agent into a three-necked flask, add 2 mL of defoamer tributyl phosphate, stir at 500 rpm, stir in a water bath at 60°C for 1...
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